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Simulation and experimental analysis of nanoscale precipitation during ageing treatment of laser powder-bed fusion fabricated IN718 Ni-based superalloy
KTH, School of Industrial Engineering and Management (ITM), Materials Science and Engineering, Structures. Isfahan Univ Technol, Dept Mat Engn, Esfahan 8415683111, Iran..ORCID iD: 0000-0001-9339-0180
KTH, School of Industrial Engineering and Management (ITM), Materials Science and Engineering.ORCID iD: 0000-0003-4351-3132
KTH, School of Industrial Engineering and Management (ITM), Materials Science and Engineering, Structures.ORCID iD: 0000-0001-8797-4585
Nucl Phys Inst, CP 130, Husinec Rez 25068, Czech Republic..
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2022 (English)In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 191, article id 112163Article in journal (Refereed) Published
Abstract [en]

Temporal evolution of the nanoscale disc-shaped gamma';'; (Ni3Nb) and spherical gamma'; (Ni3(Al,Ti)) strengthening pre-cipitates during double-stage ageing treatment of the laser powder-bed fusion (LPBF) fabricated IN718 Ni-based superalloy is studied by thermodynamic-based modeling, electron microscopy, and small-angle neutron scat-tering (SANS). The precipitation kinetics of both gamma';'; and gamma'; particles in the multi-component/multi-phase IN718 alloy system was successfully predicted by the Langer-Schwartz-Kampmann-Wagner approach. The simulated particle size and volume fraction during ageing was validated against electron microscopy and SANS results, respectively. The size and volume fraction of the gamma';'; phase was monotonically increased during the first ageing stage up to about 100 nm and 14%, respectively, but interestingly unchanged during the second stage. On the other hand, the volume fraction of gamma'; phase was sharply increased to about 15% after about 100 s and kept constant until the end of the first ageing stage, where it then decreased to about 7%. The gamma'; particle size monotonically increased up to about 20 nm. According to the determined temporal evolution of the nanoscale precipitates, a shorter ageing treatment of the LPBF IN718 superalloy compared to the conventionally manu-factured alloy could be suggested.

Place, publisher, year, edition, pages
2022. Vol. 191, article id 112163
Keywords [en]
Laser powder-bed fusion, IN718 Ni-based superalloy, Precipitation simulation, Ageing, Small-angle neutron scattering
National Category
Other Materials Engineering Metallurgy and Metallic Materials Physical Chemistry
Identifiers
URN: urn:nbn:se:kth:diva-316736DOI: 10.1016/j.matchar.2022.112163ISI: 000839364200001Scopus ID: 2-s2.0-85135141376OAI: oai:DiVA.org:kth-316736DiVA, id: diva2:1691395
Note

QC 20220830

Available from: 2022-08-30 Created: 2022-08-30 Last updated: 2023-12-07Bibliographically approved

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Kermanpur, AhmadBabu, PrasathLarsson, HenrikHedström, Peter

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