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Novel monomeric phenanthroline-thallium(III) complexes multinuclear NMR characterization in organic solvents
KTH, Tidigare Institutioner (före 2005), Kemi.
2002 (engelsk)Inngår i: Chinese Chemical Letters, ISSN 1001-8417, E-ISSN 1878-5964, Vol. 13, nr 7, s. 695-698Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

A novel complex of monomeric thallium(III) with the nitrogen donor ligand phenanthroline (phen) has been prepared and characterized by multinuclear NMR (H-1, C-13, Tl-205). The three complexes exist in equilibria in DMSO and acetonitrile solution which was proved by the Tl-205 NMR spectra. The H-1 and C-13 NMR spectra of tris-phen Tl(III) complex have been measured, where the spin-spin coupling between Tl (I = 1/2) and C-13 or H-1 signals were observed with the H-1 and C-13 NMR spectroscopy in acetonitrile. The coupling constants are presented and the chemical shifts of complexes are discussed in detail.

sted, utgiver, år, opplag, sider
2002. Vol. 13, nr 7, s. 695-698
Emneord [en]
thallium(III), phenanthroline (phen), N-donor ligands, NMR spectroscopy, aqueous-solution
Identifikatorer
URN: urn:nbn:se:kth:diva-21714ISI: 000176817000034OAI: oai:DiVA.org:kth-21714DiVA, id: diva2:340412
Merknad
QC 20100525Tilgjengelig fra: 2010-08-10 Laget: 2010-08-10 Sist oppdatert: 2022-06-25bibliografisk kontrollert

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