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HBF4 center dot DEE-catalyzed formation of sulfinyl imines: Synthesis and mechanistic studies
KTH, Skolan för kemi, bioteknologi och hälsa (CBH), Kemi.
KTH, Skolan för kemi, bioteknologi och hälsa (CBH), Kemi.ORCID-id: 0000-0001-6782-6622
2018 (engelsk)Inngår i: Tetrahedron Letters, ISSN 0040-4039, E-ISSN 1359-8562, Vol. 59, nr 13, s. 1249-1253Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

A mild acid-catalysed method is reported for the formation of sulfinyl imines from tert-butanesulfinamide and aromatic or aliphatic aldehydes using tetrafluoroboric acid diethyletherate (10 mol%) in dichloromethane. Reactions were performed at room temperature and gave the corresponding sulfinyl imines in excellent yield after 2 h. A DFT study was performed and a mechanism for the reaction is postulated. 

sted, utgiver, år, opplag, sider
PERGAMON-ELSEVIER SCIENCE LTD , 2018. Vol. 59, nr 13, s. 1249-1253
Emneord [en]
Sulfinyl imine, Bronsted acid catalysis, Tetrafluoroboric acid, Mechanistic study, DFT
HSV kategori
Identifikatorer
URN: urn:nbn:se:kth:diva-225705DOI: 10.1016/j.tetlet.2018.02.051ISI: 000428007300020Scopus ID: 2-s2.0-85042402317OAI: oai:DiVA.org:kth-225705DiVA, id: diva2:1196754
Merknad

QC 20180411, Funding Agency: KTH-Royal Institute of Technology 

Tilgjengelig fra: 2018-04-11 Laget: 2018-04-11 Sist oppdatert: 2018-04-11bibliografisk kontrollert

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