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Feasibility of monomer aromatic substances as calibration standards for lignin quantitative analyses in Pyrolysis-GCMS
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.ORCID iD: 0000-0002-2900-4713
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.ORCID iD: 0000-0002-4521-1122
2013 (English)In: Journal of Analytical and Applied Pyrolysis, ISSN 0165-2370, E-ISSN 1873-250X, Vol. 101, p. 232-237Article in journal (Refereed) Published
Abstract [en]

In this article, the feasibilities of five different monomer aromatic substances as calibration standards by analytical pyrolysis with gas chromatographic separation and mass selective detection (Py-GC/MS) were applied for the quantification of lignin in paper and pulp. The stabilities of these substances in the pyrolysis process were evaluated and the curves of peak response area to mass also were obtained. The results showed that the substances with exact same substitutions on the benzene ring as lignin units had good stabilities in the pyrolysis process with good lineabilities of peak response area to the mass curves, which implicated these substances can be applied as calibration standards in the liginin quick quantitative analyse without tedious pretreatments and structure changes.

Place, publisher, year, edition, pages
2013. Vol. 101, p. 232-237
Keywords [en]
Lignin unit, Calibration standards, Pyrolysis-GC-MS, Quantitative analyse
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Identifiers
URN: urn:nbn:se:kth:diva-123421DOI: 10.1016/j.jaap.2012.12.015ISI: 000318380800029Scopus ID: 2-s2.0-84876183023OAI: oai:DiVA.org:kth-123421DiVA, id: diva2:626702
Note

QC 20130610

Available from: 2013-06-10 Created: 2013-06-10 Last updated: 2024-03-18Bibliographically approved

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Lindström, Mikael E.Li, Jiebing

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