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Combined ion micro probe and SEM analysis of strongly non uniform deposits in fusion devices
KTH, Skolan för elektro- och systemteknik (EES), Fusionsplasmafysik.
KTH, Skolan för elektro- och systemteknik (EES), Fusionsplasmafysik.
KTH, Skolan för elektro- och systemteknik (EES), Fusionsplasmafysik.
Vise andre og tillknytning
2015 (engelsk)Inngår i: Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, ISSN 0168-583X, E-ISSN 1872-9584, Vol. 342, s. 19-28Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

Conventional ion beam analysis (IBA) of deposited layers from fusion devices may have insufficient accuracy due to strongly uneven appearance of the layers. Surface roughness and spatial variation of the matrix composition make interpretation of broad beam spectra complex and non obvious. We discuss complications of applied IBA arising for fusion-relevant surfaces and demonstrate how quantification can be improved by employing micro IBA methods. The analysis is bound to pre-defined regions on the sample surface and can be extended by employing beams of several types, scanning electron microscopy (SEM) and stereo SEM techniques.

sted, utgiver, år, opplag, sider
2015. Vol. 342, s. 19-28
Emneord [en]
Ion micro probe, Micro NRA, PIXE, Plasma-facing components, Deuterium retention
HSV kategori
Identifikatorer
URN: urn:nbn:se:kth:diva-145076DOI: 10.1016/j.nimb.2014.08.019ISI: 000347770500004OAI: oai:DiVA.org:kth-145076DiVA, id: diva2:716165
Merknad

Updated from submitted to published.

QC 20150227

Tilgjengelig fra: 2014-05-08 Laget: 2014-05-08 Sist oppdatert: 2017-12-05bibliografisk kontrollert
Inngår i avhandling
1. Experimental studies of materials migration in magnetic confinement fusion devices: Novel methods for measurement of macro particle migration, transport of atomic impurities and characterization of exposed surfaces
Åpne denne publikasjonen i ny fane eller vindu >>Experimental studies of materials migration in magnetic confinement fusion devices: Novel methods for measurement of macro particle migration, transport of atomic impurities and characterization of exposed surfaces
2014 (engelsk)Doktoravhandling, med artikler (Annet vitenskapelig)
Abstract [en]

During several decades of research and development in the field of Magnetically Confined Fusion (MCF) the preferred selection of materials for Plasma Facing Components (PFC) has changed repeatedly. Without doubt, endurance of the first wall will decide research availability and lifespan of the first International Thermonuclear Research Reactor (ITER). Materials erosion, redeposition and mixing in the reactor are the critical processes responsible for modification of materials properties under plasma impact. This thesis presents several diagnostic techniques and their applications for studies of materials transport in fusion devices. The measurements were made at the EXTRAP T2R Reversed Field Pinch operated in Alfvén laboratory at KTH (Sweden), the TEXTOR tokamak, recently shut down at Forschungszentrum Jülich (Germany) and in the JET tokamak at CCFE (UK). The main outcomes of the work are:

  • Development and application of a method for non-destructive capture and characterization of fast dust particles moving in the edge plasma of fusion devices, as well as particles generated upon laser-assisted cleaning of plasma exposed surfaces. 
  • Advancement of conventional broad beam and micro ion beam techniques to include measurement of tritium in the surfaces exposed in future D-T experiments. 
  • Adaption of the micro ion beam method for precision mapping of non uniform elements concentrations on irregular surfaces. 
  • Implementation of an isotopic marker to study the large scale materials migration in a tokamak and development of a method for fast non destructive sampling of the marker on surfaces of PFCs.
sted, utgiver, år, opplag, sider
Stockholm: KTH Royal Institute of Technology, 2014. s. iv, 84
Serie
TRITA-EE, ISSN 1653-5146 ; 2014:024
Emneord
fusion, tokamak, RFP, divertor, limiter, SOL, transport, migration, surface analysis, IBA, ion micro beam, beryllium, tritium
HSV kategori
Forskningsprogram
Fysik
Identifikatorer
urn:nbn:se:kth:diva-145045 (URN)978-91-7595-147-8 (ISBN)
Disputas
2014-05-16, F3, Lindstedsvägen 26, KTH, Stockholm, 14:00 (engelsk)
Opponent
Veileder
Merknad

QC 20140508

Tilgjengelig fra: 2014-05-08 Laget: 2014-05-07 Sist oppdatert: 2014-05-08bibliografisk kontrollert

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