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Investigating Polymer-Metal Interfaces by Grazing Incidence Small-Angle X-Ray Scattering from Gradients to Real-Time Studies
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
2016 (English)In: NANOMATERIALS, ISSN 2079-4991, Vol. 6, no 12, 239Article, review/survey (Refereed) Published
Abstract [en]

Tailoring the polymer-metal interface is crucial for advanced material design. Vacuum deposition methods for metal layer coating are widely used in industry and research. They allow for installing a variety of nanostructures, often making use of the selective interaction of the metal atoms with the underlying polymer thin film. The polymer thin film may eventually be nanostructured, too, in order to create a hierarchy in length scales. Grazing incidence X-ray scattering is an advanced method to characterize and investigate polymer-metal interfaces. Being non-destructive and yielding statistically relevant results, it allows for deducing the detailed polymer-metal interaction. We review the use of grazing incidence X-ray scattering to elucidate the polymer-metal interface, making use of the modern synchrotron radiation facilities, allowing for very local studies via in situ (so-called stop-sputter) experiments as well as studies observing the nanostructured metal nanoparticle layer growth in real time.

Place, publisher, year, edition, pages
2016. Vol. 6, no 12, 239
Keyword [en]
polymer-metal interfaces, nanocomposites, nanostructure formation, sputter deposition, polymer template, X-ray scattering, grazing incidence X-ray scattering, in situ, growth kinetics
National Category
Nano Technology
Identifiers
URN: urn:nbn:se:kth:diva-202453DOI: 10.3390/nano6120239ISI: 000392240000018Scopus ID: 2-s2.0-85010299059OAI: oai:DiVA.org:kth-202453DiVA: diva2:1078591
Note

QC 20170306

Available from: 2017-03-06 Created: 2017-03-06 Last updated: 2017-03-07Bibliographically approved

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