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Fully bio-based aliphatic thermoset polyesters via self-catalyzed self-condensation of multifunctional epoxy monomers directly extracted from natural sources
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Coating Technology.
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Coating Technology.
2017 (English)In: Journal of Coatings Technology Research, ISSN 1945-9645, Vol. 14, no 4, 757-765 p.Article in journal (Refereed) Published
Abstract [en]

The use of bio-based raw material is regarded as a sustainable way to address environmental concerns. A naturally occurring monomer, 9,10-epoxy-18-hydroxyoctadecanoic acid (EFA), was retrieved from outer birch bark. A series of model experiments revealing relative reaction rates for epoxide, carboxylic acid, and alcohol functional groups was investigated. Real-time Fourier transform infrared spectroscopy and nuclear magnetic resonance were used to follow the different model experiments. The results on the model systems were then compared to the thermoset formation of thermally cured EFA. Finally, the adhesive properties of crosslinked EFA on different substrates were evaluated.

Place, publisher, year, edition, pages
Springer, 2017. Vol. 14, no 4, 757-765 p.
Keyword [en]
Bio-based monomer, Epoxide, Self-catalysis, Thermoset
National Category
Polymer Technologies
Identifiers
URN: urn:nbn:se:kth:diva-212949DOI: 10.1007/s11998-017-9920-yISI: 000406744400002Scopus ID: 2-s2.0-85016397686OAI: oai:DiVA.org:kth-212949DiVA: diva2:1136063
Conference
12th Coatings Science International Conference (COSI), JUN 27-JUL 01, 2016, Noordwijk, Netherlands
Funder
Swedish Research Council Formas, 211-2013-70
Note

QC 20170825

Available from: 2017-08-25 Created: 2017-08-25 Last updated: 2017-08-25Bibliographically approved

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CiteExportLink to record
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