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Portable mini-chamber for temperature dependent studies using small angle and wide angle x-ray scattering
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2018 (English)In: DAE Solid State Physics Symposium 2017, American Institute of Physics (AIP), 2018, Vol. 1942, article id 080057Conference paper, Published paper (Refereed)
Abstract [en]

The present work describes the design and performance of a vacuum compatible portable mini chamber for temperature dependent GISAXS and GIWAXS studies of thin films and multilayer structures. The water cooled body of the chamber allows sample annealing up to 900 K using ultra high vacuum compatible (UHV) pyrolytic boron nitride heater, thus making it possible to study the temperature dependent evolution of structure and morphology of two-dimensional nanostructured materials. Due to its light weight and small size, the chamber is portable and can be accommodated at synchrotron facilities worldwide. A systematic illustration of the versatility of the chamber has been demonstrated at beamline P03, PETRA-III, DESY, Hamburg, Germany. Temperature dependent grazing incidence small angle x-ray scattering (GISAXS) and grazing incidence wide angle x-ray scattering (GIWAXS) measurements were performed on oblique angle deposited Co/Ag multilayer structure, which jointly revealed that the surface diffusion in Co columns in Co/Ag multilayer enhances by increasing temperature from RT to ∼573 K. This results in a morphology change from columnar tilted structure to densely packed morphological isotropic multilayer

Place, publisher, year, edition, pages
American Institute of Physics (AIP), 2018. Vol. 1942, article id 080057
Series
AIP Conference Proceedings, ISSN 0094-243X ; 1942
National Category
Materials Chemistry
Identifiers
URN: urn:nbn:se:kth:diva-227618DOI: 10.1063/1.5028891ISI: 000433118300312Scopus ID: 2-s2.0-85045731730ISBN: 9780735416345 (print)OAI: oai:DiVA.org:kth-227618DiVA, id: diva2:1206546
Conference
62nd DAE Solid State Physics Symposium 2017, 26 December 2017 through 30 December 2017, Mumbai, India
Note

QC 20180517

Available from: 2018-05-17 Created: 2018-05-17 Last updated: 2019-08-30Bibliographically approved

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CiteExportLink to record
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Citation style
  • apa
  • harvard1
  • ieee
  • modern-language-association-8th-edition
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  • nn-NB
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  • Other locale
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Output format
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