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Zirconium catalyzed amide formation without water scavenging
KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemistry, Organic chemistry.ORCID iD: 0000-0002-4704-1892
Stockholm Univ, Dept Organ Chem, Arrhenius Lab, SE-10691 Stockholm, Sweden..
Umea Univ, Dept Chem, SE-90187 Umea, Sweden..
2019 (English)In: Applied organometallic chemistry, ISSN 0268-2605, E-ISSN 1099-0739, article id e5062Article in journal (Refereed) Epub ahead of print
Abstract [en]

A scalable homogeneous metal-catalyzed protocol for direct amidation of carboxylic acids is presented. The use of 2-10 mol% of the commercially available Zr(Cp)(2)(OTf)(2)center dot THF results in high yields of amides at moderate temperature, using an operationally convenient reaction protocol that circumvents the use of water scavenging techniques.

Place, publisher, year, edition, pages
Wiley , 2019. article id e5062
Keywords [en]
mides, amines, carboxylic acids, catalysis, direct amidation, trifluoromethanesulfonate, zirconium
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-255556DOI: 10.1002/aoc.5062ISI: 000476374900001Scopus ID: 2-s2.0-85069697551OAI: oai:DiVA.org:kth-255556DiVA, id: diva2:1341316
Note

QC 20190808

Available from: 2019-08-08 Created: 2019-08-08 Last updated: 2019-10-04Bibliographically approved

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