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Synthesis of 2H‐pyrano[2,3‐b]quinolines. Part II. Preparation and 1H‐nmr investigations of 4‐hydroxy‐2‐methyl‐3,4‐dihydro‐2H‐pyrano[2,3‐b]quinolines
Alkaloida Chemical Company Ltd., Tiszavasvari, H-4440, Hungary.ORCID iD: 0000-0002-7552-1076
1995 (English)In: Journal of Heterocyclic Chemistry, ISSN 0022-152X, E-ISSN 1943-5193, Vol. 32, no 3, p. 755-760Article in journal (Refereed) Published
Abstract [en]

Diastereoisomers of 4‐hydroxy‐2‐methyl‐3,4‐dihydro‐2H‐pyrano[2,3‐b]quinolines 8 and 9 were synthesized starting from the appropriate 2‐chloroquinoline‐3‐carboxaldehydes 1. The relative configuration of the 1,3‐diol intermediates 4 and 5 was determined on the basis of the 13C‐nmr spectra of their acetonides. The relative stereochemistry of title compounds was confirmed by using homonuclear NOE and selective decoupling experiments, as well as by analysis of the coupling patterns observed in their 1H‐nmr spectra. 

Place, publisher, year, edition, pages
Wiley , 1995. Vol. 32, no 3, p. 755-760
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-317916DOI: 10.1002/jhet.5570320311ISI: A1995RG03800011Scopus ID: 2-s2.0-84993924924OAI: oai:DiVA.org:kth-317916DiVA, id: diva2:1695809
Note

QC 20220915

Available from: 2022-09-14 Created: 2022-09-14 Last updated: 2022-09-15Bibliographically approved

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Szabó, Zoltan

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