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Fused 1,2,4-TriazoIe Heterocycles. IV. Synthesis of Four New Heterocyclic Ring Systems of [1,2,4]Triazolo[1,3]thiazinoquinolines
KTH, Superseded Departments (pre-2005), Chemistry.ORCID iD: 0000-0002-7552-1076
1997 (English)In: Journal of Heterocyclic Chemistry, ISSN 0022-152X, E-ISSN 1943-5193, Vol. 34, no 4, p. 1275-1281Article in journal (Refereed) Published
Abstract [en]

Syntheses of 5H-[1,2,4]triazolo[5′1′:2,3][1,3]thiazino[5,4-c]quinolines 8, 5H-[1,2,4]triazolo[3′,4′:2,3][1,3]thiazino[5,4-c]quinolines 9, 5H-[1,2,4]triazolo[5′1′:2,3][1,3]thiazino[5,6-c]quinolines 14 and 5H-[1,2,4]triazolo[3′,4′:2,3][1,3]thiazino[5,6-c]quinolines 15 are described starting from 4-chloro-3-chloromethylquinaldine (4) and 1,2,4-triazole-5-thiols 5 taking advantage of different reactivity of the chlorine atoms of 4 under different reaction conditions. The structures of products 8, 9, 14 and 15 and the intermediates leading to them were confirmed by desulfurization, unequivocal syntheses and nmr spectroscopy as well.

Place, publisher, year, edition, pages
Wiley , 1997. Vol. 34, no 4, p. 1275-1281
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-317904DOI: 10.1002/jhet.5570340431ISI: A1997XX67900031Scopus ID: 2-s2.0-1542675245OAI: oai:DiVA.org:kth-317904DiVA, id: diva2:1695821
Note

QC 20220915

Available from: 2022-09-14 Created: 2022-09-14 Last updated: 2022-09-15Bibliographically approved

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Szabó, Zoltan

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