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Characterization of the nature and morphology of coarse precipitation in various oxide dispersion strengthened steels
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2021 (English)In: Materialia, ISSN 2589-1529, Vol. 17, article id 101117Article in journal (Refereed) Published
Abstract [en]

Oxide Dispersion Strengthened (ODS) steels are candidate materials for both fission and fusion nuclear reactors. In this study, the microstructure of ferritic (Fe-14Cr-1W) and ferritic / martensitic (Fe-9Cr-1W) ODS steels has been characterized after two different processing routes: Hot Extrusion (HE) and Hot Isostatic Pressing (HIP). Transmission Kikuchi Diffraction (TKD) revealed the presence of Ti-rich precipitates on every specimen. They are identified by X-Ray Diffraction (XRD) as Ti(C,N) and Ti-O (Ti2O3 or TiO2). Intergranular M7C3 and M23C6 have been observed on most Fe-14Cr ODS steels except one, where no Cr-carbides have been found. In Fe-9Cr ODS, intergranular Cr-rich M23C6 carbides have been found. The lack of M7C3 on Fe-9Cr ODS is possibly linked to the matrix phase transformation, not occurring in the Fe-14Cr ODS. Cr-carbides display highly elongated shapes for the Fe-14Cr HE specimens that could be detrimental to the mechanical behavior of the material.

Place, publisher, year, edition, pages
Elsevier BV , 2021. Vol. 17, article id 101117
Keywords [en]
Carbides, Nitrides, Oxide dispersion strengthened (ODS) steel, Precipitation, Transmission Kikuchi Diffraction (TKD), X-Ray Diffraction (XRD)
National Category
Metallurgy and Metallic Materials
Identifiers
URN: urn:nbn:se:kth:diva-343626DOI: 10.1016/j.mtla.2021.101117ISI: 000669505500008Scopus ID: 2-s2.0-85106958042OAI: oai:DiVA.org:kth-343626DiVA, id: diva2:1839748
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QC 20240222

Available from: 2024-02-21 Created: 2024-02-21 Last updated: 2024-02-22Bibliographically approved

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Spartacus, Gabriel

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Spartacus, GabrielMenut, DenisToffolon-Masclet, CarolineSornin, Denis
Metallurgy and Metallic Materials

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CiteExportLink to record
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Citation style
  • apa
  • ieee
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  • de-DE
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