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Quantitative determination of volatiles in polymers and quality control of recycled materials by static headspace techniques
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.ORCID iD: 0000-0002-7790-8987
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
2008 (English)In: CHROMATOGRAPHY FOR SUSTAINABLE POLYMERIC MATERIALS: RENEWABLE, DEGRADABLE AND RECYCLABLE, Berlin: Springer Verlag , 2008, Vol. 211, 51-84 p.Chapter in book (Refereed)
Abstract [en]

A presentation is given of headspace (HS) extraction and headspace solid-phase microextraction (HS-SPME) techniques and their combination with multiple headspace (MHS) extraction to enable quantitative determination of volatiles in solid polymer matrixes. As an example, the development of HS, HS-SPME, and MHS-SPME methods for extraction of volatiles from thermo-oxidized and/or recycled polyamide 6.6 is reviewed with special focus on the problems encountered when extracting analytes from solid-sample matrixes including excessively long equilibrium times and adsorption of analytes to the sample matrix. Examples are also given of the application of HS-SPME in quality control of recycled materials, in durability assessment of polymeric materials and in degradation studies.

Place, publisher, year, edition, pages
Berlin: Springer Verlag , 2008. Vol. 211, 51-84 p.
, Advances in Polymer Science, ISSN 00653195 ; 211
Keyword [en]
degradation, multiple headspace extraction, quality control, recycling, solid-phase microextraction, solid-phase microextraction, chromatography-mass-spectrometry, phenolic, prepreg waste, fiberglass reinforced polyamide-66, accelerated, solvent-extraction, capillary gas-chromatography, head-space analysis, dynamic headspace, packaging materials, mechanical-properties
National Category
Polymer Technologies Polymer Chemistry
URN: urn:nbn:se:kth:diva-17695DOI: 10.1007/12_2007_117ISI: 000257692200003ScopusID: 2-s2.0-54249115115ISBN: 978-354078762-4OAI: diva2:335740

QC 20150622

Available from: 2010-08-05 Created: 2010-08-05 Last updated: 2015-06-22Bibliographically approved

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Gröning, MikaelHakkarainen, MinnaAlbertsson, Ann-Christine
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