Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • harvard1
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
CTAB-Mn3O4 nanocomposites: Synthesis, NMR and low temperature EPR studies
Show others and affiliations
2010 (English)In: Polyhedron, ISSN 0277-5387, E-ISSN 1873-3719, Vol. 29, no 5, 1375-1380 p.Article in journal (Refereed) Published
Abstract [en]

We are reporting on the synthesis of Mn3O4 nanoparticles and CTAB-Mn3O4 nanocomposites via a sonochemical route using MnCl2, ethanol, NaOH and CTAB. The crystalline phase was identified as Mn3O4. The crystallite size of the CTAB-Mn3O4 nanocomposite was identified as 13 +/- 5 nm from X-ray line profile fitting and the particle size from TEM was 107.5 +/- 1.4 nm. The interaction between CEAB and the Mn3O4 nanoparticles was investigated by FTIR and H-1 NMR spectroscopies. Two different magnetic phase transitions were observed for both samples below the Curie temperature (43 degrees C) by using a low temperature Electron Paramagnetic Resonance (EPR) technique. Also we determined the effect of the capping with CTAB on the reduction in absorbed power.

Place, publisher, year, edition, pages
2010. Vol. 29, no 5, 1375-1380 p.
Keyword [en]
Nanostructures, Sonochemical synthesis, Nanocomposite, Mn3O4, NMR, EPR, mn3o4 nanocrystallites, magnetic-properties, nanoparticles, irradiation, nanorods, hausmannite, monolayers, nanowires, complex
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-19400DOI: 10.1016/j.poly.2009.12.034ISI: 000276720400001Scopus ID: 2-s2.0-77649274994OAI: oai:DiVA.org:kth-19400DiVA: diva2:337447
Funder
Knut and Alice Wallenberg Foundation
Note
QC 20100525Available from: 2010-08-05 Created: 2010-08-05 Last updated: 2017-12-12Bibliographically approved

Open Access in DiVA

No full text

Other links

Publisher's full textScopus

Authority records BETA

Toprak, Muhammet S.

Search in DiVA

By author/editor
Toprak, Muhammet S.
By organisation
Functional Materials, FNM
In the same journal
Polyhedron
Chemical Sciences

Search outside of DiVA

GoogleGoogle Scholar

doi
urn-nbn

Altmetric score

doi
urn-nbn
Total: 63 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • harvard1
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf