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Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences
2003 (English)In: Journal of magnetic resonance, ISSN 1090-7807, E-ISSN 1096-0856, Vol. 164, no 1, 165-170 p.Article in journal (Refereed) Published
Abstract [en]

A pulse sequence is described for the recoupling of heteronuclear dipolar interactions under MAS. The method is similar to the PISEMA experiment, but employs a well-defined amplitude modulation of one of the two radio-frequency fields. The technique is used for measurements of H-1-C-13 dipolar couplings in unoriented solid and liquid-crystalline samples.

Place, publisher, year, edition, pages
2003. Vol. 164, no 1, 165-170 p.
Keyword [en]
heteronuclear recoupling, magic-angle spinning, cross-polarization, PISEMA, liquid crystals, state nmr-spectroscopy, inversion spin-exchange, nuclear-magnetic-resonance, magic-angle nmr, cross-polarization, chemical-shift, orientational constraints, membrane-proteins, rotating solids, lipid bilayers
Identifiers
URN: urn:nbn:se:kth:diva-22780DOI: 10.1016/s1090-7807(03)00180-0ISI: 000185095200021OAI: oai:DiVA.org:kth-22780DiVA: diva2:341478
Note
QC 20100525Available from: 2010-08-10 Created: 2010-08-10 Last updated: 2017-12-12Bibliographically approved

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Dvinskikh, Sergey V.

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