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Synthesis and crystal structure of Fe(CP)(2) (3)(Bi2Cl9)center dot thf
KTH, Superseded Departments, Chemistry.
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2003 (English)In: Zeitschrift für Anorganische und Allgemeines Chemie, ISSN 0044-2313, E-ISSN 1521-3749, Vol. 629, no 14, 2525-2528 p.Article in journal (Refereed) Published
Abstract [en]

Single crystals of [Fe(CP)(2)](3)(Bi2Cl9)(.)thf were obtained from a thf solution containing ferrocene and BiCl3. The structure shows disorder at room temperature which disappears upon cooling, coupled with a decrease in symmetry. The title compound crystallizes in the orthorhombic space group P2(1)2(1)2(1) [a = 1698.64(2), b = 2318.69(3), c = 1085.66(2) pm] with three ferrocenium ions, one nonachlorodibismutate ion and one molecule of thf in the asymmetric unit.

Place, publisher, year, edition, pages
2003. Vol. 629, no 14, 2525-2528 p.
Keyword [en]
ferrocenium, chlorobismutate, Raman spectroscopy, crystal structure, ferrocene
Identifiers
URN: urn:nbn:se:kth:diva-23096DOI: 10.1002/zaac.200300289ISI: 000188203600020OAI: oai:DiVA.org:kth-23096DiVA: diva2:341794
Note
QC 20100525Available from: 2010-08-10 Created: 2010-08-10 Last updated: 2017-12-12Bibliographically approved

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Kloo, Lars A.Fischer, Andreas
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