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Synthesis and crystal structures of new palladium(II) - Gallium(III) complexes with bridging halogenide ligands
KTH, Superseded Departments, Chemistry.
KTH, Superseded Departments, Chemistry.
KTH, Superseded Departments, Chemistry.
2004 (English)In: Zeitschrift für Anorganische und Allgemeines Chemie, ISSN 0044-2313, E-ISSN 1521-3749, Vol. 630, no 2, 324-326 p.Article in journal (Refereed) Published
Abstract [en]

The reaction of palladium(H) bromide or palladium(II) iodide with the respective gallium(III) halogenide in the presence of aromatic solvents leads to the formation of palladium(II) tetrabromo- and tetraiodogallate. The compounds are isostructural {monoclinic, C2/m, Pd[GaBr4](2): a=1267(2), b=808(1), c=722(1) pm, beta=94.5(1)degrees; Pd[GaI4](2): a=1363(1), b=849.9(4), c=756.6(7) pm, beta=95.38(3)degrees}. The structures contain mononuclear complexes Pd[GaX4](2), where X- = Br- (1), I- (2). The crystal structures of 1 and 2 were determined by single-crystal X-ray diffraction. Crystals of both compounds turned out to be similarly twinned.

Place, publisher, year, edition, pages
2004. Vol. 630, no 2, 324-326 p.
Keyword [en]
palladium, gallium, crystal structures, arenes, vapor complex, aluminum
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:kth:diva-23197DOI: 10.1002/zaac.200300339ISI: 000189145800025Scopus ID: 2-s2.0-1242329281OAI: oai:DiVA.org:kth-23197DiVA: diva2:341895
Note
QC 20100525 QC 20111031Available from: 2010-08-10 Created: 2010-08-10 Last updated: 2017-12-12Bibliographically approved

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