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On experimental aspects of electrophoretic NMR
KTH, Superseded Departments, Chemistry.
KTH, Superseded Departments, Chemistry. KTH, Superseded Departments, Physics.ORCID iD: 0000-0002-0231-3970
KTH, Superseded Departments, Chemistry.
2004 (English)In: Concepts in magnetic resonance. Bridging education and research, ISSN 1546-6086, E-ISSN 1552-5023, Vol. 22, no 2, 61-68 p.Article in journal (Refereed) Published
Abstract [en]

Artefacts in electrophoretic NMR experiments are investigated in detail. We identify electroosmosis, sample heating, and gas development on the electrodes as main error sources and suggest experimental strategies and setups to suppress their influence on the monitored electrophoretic mobilities. We hereby demonstrate essentially artefact-free experiments up to currents and electric fields 3 mA and 70 V/cm, respectively.

Place, publisher, year, edition, pages
2004. Vol. 22, no 2, 61-68 p.
Keyword [en]
electrophoretic NMR, pulsed field gradient, electrophoresis, electromigration, stimulated echo, pulse sequence, electric field, sample heating, electroosmosis, coating, Pt black, electrolysis, polyelectrolyte, ionic strength, charged particle, capillary-zone-electrophoresis, nuclear magnetic-resonance, diffusion measurements, electroosmotic flow, surfactant systems, temperature, convection, field, suppression, buffer
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-23574DOI: 10.1002/cmr.a.20012ISI: 000222647800001Scopus ID: 2-s2.0-17444401578OAI: oai:DiVA.org:kth-23574DiVA: diva2:342272
Note
QC 20100525 QC 20111103Available from: 2010-08-10 Created: 2010-08-10 Last updated: 2017-12-12Bibliographically approved

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Furo, Istvan

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