Nanocrystallinity in RuO2 coatings-Influence of precursor and preparation temperature
2010 (English)In: Thin Solid Films, ISSN 0040-6090, E-ISSN 1879-2731, Vol. 518, no 14, 3615-3618 p.Article in journal (Refereed) Published
The effects of precursor and calcination temperature on the nano morphology of ruthenium dioxide on titanium, prepared from thermal decomposition of aqueous salt solutions were investigated. Transmission electron microscopy. X-ray diffraction, gas porosimetry and cyclic voltammetry showed that lower calcination temperature yielded smaller crystallites. The crystallites were between 6 and 22 nm in diameter. When using ruthenium nitrosyl nitrate the firing temperature had a large impact on the grain size, but for chloride there was only a minor effect in the temperature range 350-550 degrees C.
Place, publisher, year, edition, pages
2010. Vol. 518, no 14, 3615-3618 p.
Ruthenium nitrosyl nitrate, Crystallization, X-ray diffraction, Catalysis, Annealing
Chemical Engineering Materials Engineering
IdentifiersURN: urn:nbn:se:kth:diva-27558DOI: 10.1016/j.tsf.2009.09.065ISI: 000278064600004ScopusID: 2-s2.0-77950543416OAI: oai:DiVA.org:kth-27558DiVA: diva2:378731
QC 201012162010-12-162010-12-132010-12-16Bibliographically approved