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Nanocrystallinity in RuO2 coatings-Influence of precursor and preparation temperature
KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry.ORCID iD: 0000-0001-5816-2924
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2010 (English)In: Thin Solid Films, ISSN 0040-6090, E-ISSN 1879-2731, Vol. 518, no 14, 3615-3618 p.Article in journal (Refereed) Published
Abstract [en]

The effects of precursor and calcination temperature on the nano morphology of ruthenium dioxide on titanium, prepared from thermal decomposition of aqueous salt solutions were investigated. Transmission electron microscopy. X-ray diffraction, gas porosimetry and cyclic voltammetry showed that lower calcination temperature yielded smaller crystallites. The crystallites were between 6 and 22 nm in diameter. When using ruthenium nitrosyl nitrate the firing temperature had a large impact on the grain size, but for chloride there was only a minor effect in the temperature range 350-550 degrees C.

Place, publisher, year, edition, pages
2010. Vol. 518, no 14, 3615-3618 p.
Keyword [en]
Ruthenium nitrosyl nitrate, Crystallization, X-ray diffraction, Catalysis, Annealing
National Category
Chemical Engineering Materials Engineering
Identifiers
URN: urn:nbn:se:kth:diva-27558DOI: 10.1016/j.tsf.2009.09.065ISI: 000278064600004Scopus ID: 2-s2.0-77950543416OAI: oai:DiVA.org:kth-27558DiVA: diva2:378731
Note
QC 20101216Available from: 2010-12-16 Created: 2010-12-13 Last updated: 2017-12-11Bibliographically approved

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Cornell, Ann

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