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Synthesis of Benzotriazine and Aryltriazene Derivatives Starting from 2-Azidobenzonitrile Derivatives
KTH, School of Chemical Science and Engineering (CHE), Chemistry, Inorganic Chemistry.
2010 (English)In: European Journal of Organic Chemistry, ISSN 1434-193X, E-ISSN 1099-0690, no 34, 6588-6599 p.Article in journal (Refereed) Published
Abstract [en]

3-Substituted 3,4-dihydro-4-imino-1,2,3-benzotriazine derivatives 7 were formed from 2-azidobenzonitriles 4 as starting materials on treatment with Grignard or lithium organic reagents. In some cases these procedures gave aryltriazenes 10 and 11 as products. All compounds were identified by NMR spectroscopy and the structures of three products, namely 7a, 10a and 11i, were corroborated by X-ray crystallography.

Place, publisher, year, edition, pages
2010. no 34, 6588-6599 p.
Keyword [en]
Nitrogen heterocycles, Grignard reaction, Substituent effects, Azides, Nitriles
National Category
Organic Chemistry
Identifiers
URN: urn:nbn:se:kth:diva-28598DOI: 10.1002/ejoc.201000328ISI: 000285262700013Scopus ID: 2-s2.0-78649533140OAI: oai:DiVA.org:kth-28598DiVA: diva2:388085
Note
QC 20110117Available from: 2011-01-17 Created: 2011-01-17 Last updated: 2017-12-11Bibliographically approved

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