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Copper-catalyzed synthesis of N-sulfonyl-1,2,3-triazoles: Controlling selectivity
Department of Chemistry, Building 201, Kemitorvet Technical University of Denmark.ORCID iD: 0000-0002-1553-4027
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2007 (English)In: Angewandte Chemie International Edition, ISSN 1433-7851, E-ISSN 1521-3773, Vol. 46, no 10, 1730-1733 p.Article in journal (Refereed) Published
Abstract [en]

(Chemical Equation Presented) 4-Substituted 1-(N-sulfonyl)-1,2,3-triazoles are selectively obtained by using the Cu-catalyzed azide-alkyne cycloaddition reaction with sulfonyl azides. Performing the reaction at 0°C in chloroform in the presence of 2,6-lutidine and Cul as the catalyst effectively prevents the ketenimine pathway and provides convenient access to N-sulfonyltriazoles in good to excellent yields.

Place, publisher, year, edition, pages
2007. Vol. 46, no 10, 1730-1733 p.
Keyword [en]
alkynes, copper, cycloaddition, sulfonyl azides, sulfonyltriazoles
National Category
Organic Chemistry
Identifiers
URN: urn:nbn:se:kth:diva-48880DOI: 10.1002/anie.200604241ISI: 000244698600036OAI: oai:DiVA.org:kth-48880DiVA: diva2:488409
Note
QC 20120202Available from: 2012-02-01 Created: 2011-11-23 Last updated: 2017-12-08Bibliographically approved

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Ahlquist, Mårten

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