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Measurement of Inclusion Size by Laser Ablation ICP Mass Spectrometry
Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Japan.
Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Japan.
2004 (English)In: ISIJ International, ISSN 0915-1559, E-ISSN 1347-5460, Vol. 44, no 2, 356-363 p.Article in journal (Refereed) Published
Abstract [en]

By using laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), the measurement of particle size has been made for one component oxide (Al2O3 and MgO) and multicomponent oxide (12CaO.7Al(2)O(3) and CaO-Al2O3-Mgo) located on surface of iron or glass sample, The method of particle size estimation by LA-ICP-MS has been developed coupled with a new method of making samples with particles. The size calibration lines for Al2O3, MgO and CaO particles have been obtained. The results of particle size measurement by LA-ICP-MS are compared with those by SEM and single-particle optical sensing (SPOS) methods. It was confirmed that LA-ICP-MS has the perspective to be used for the quick measurement of inclusion composition and size in metal and other materials. The size frequency distributions of Al2O3 particles measured by LA-ICP-MS in iron samples with particles agree reasonably well with those by SEM and SPOS in the range of particle diameter from 2 to 20 mum. The size of Al2O3, MgO and complex oxide (12CaO.7Al(2)O(3) and CaO-Al2O3-Mgo) particles measured by LA-ICP-MS is in good agreement with that by SEM in the range of particle diameter from 10 to 40 mum.

Place, publisher, year, edition, pages
2004. Vol. 44, no 2, 356-363 p.
National Category
Engineering and Technology
Identifiers
URN: urn:nbn:se:kth:diva-86383DOI: 10.2355/isijinternational.44.356ISI: 000220206600019OAI: oai:DiVA.org:kth-86383DiVA: diva2:500677
Note
QC 20120228Available from: 2012-02-13 Created: 2012-02-13 Last updated: 2017-12-07Bibliographically approved

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Karasev, Andrey Vladimirovich
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CiteExportLink to record
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