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A Green Chemical Synthesis and Characterization of Mn3O4 nanoparticles
Fatih Univ, Istanbul, Turkey.
Fatih Univ, Istanbul, Turkey.
KTH, School of Information and Communication Technology (ICT), Material Physics, Functional Materials, FNM.ORCID iD: 0000-0001-5678-5298
Natl Metrol Inst, Gebze, Turkey.
2012 (English)In: JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM, ISSN 1557-1939, Vol. 25, no 5, 1535-1539 p.Article in journal (Refereed) Published
Abstract [en]

Mn3O4 nanoparticles were synthesized via an ionic liquid (IL) assisted process at room temperature, which is rather difficult to achieve by other techniques. The synthesized product was characterized by powder X-ray diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, thermal gravimetry (TG), and vibrating sample magnetometry (VSM). The prepared material showed a high purity, while crystallite size and particle size agree well with each other, 17 +/- 2 and 19 +/- 3 nm, respectively, revealing nearly single crystalline character of nanoparticles. The product contains 4 wt% of adsorbed water and ionic liquid. This method provides a facile, one-step, and low-cost route for the synthesis of nanostructures of metal oxides. In addition, [BMIM]BF4 could be collected and reused for subsequent reactions.

Place, publisher, year, edition, pages
2012. Vol. 25, no 5, 1535-1539 p.
Keyword [en]
Green synthesis, Mn3O4, Magnetic nanomaterials, Room temperature ionic liquids
National Category
Condensed Matter Physics
Identifiers
URN: urn:nbn:se:kth:diva-99065DOI: 10.1007/s10948-012-1451-2ISI: 000305523100055Scopus ID: 2-s2.0-84864583017OAI: oai:DiVA.org:kth-99065DiVA: diva2:541563
Note
QC 20120719Available from: 2012-07-19 Created: 2012-07-13 Last updated: 2012-07-19Bibliographically approved

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Toprak, Muhammet S.

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