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Thermometric study of CO2-laser heated optical fibers in excess of 1700 degrees C using fiber Bragg gratings
KTH, School of Engineering Sciences (SCI), Applied Physics, Laser Physics.
KTH, School of Engineering Sciences (SCI), Applied Physics, Laser Physics.ORCID iD: 0000-0002-9207-4183
2013 (English)In: Journal of the Optical Society of America. B, Optical physics, ISSN 0740-3224, E-ISSN 1520-8540, Vol. 30, no 7, 1835-1842 p.Article in journal (Refereed) Published
Abstract [en]

The thermal response of optical fibers during CO2 laser irradiation has been characterized by using thermally stable short-period fiber Bragg gratings, referred to as chemical composition gratings. CO2 laser beam profiling was performed by scanning the beam across a 1 mm long grating, providing a spatial resolution given by the fiber diameter. The thermal dynamics during square pulse irradiation has been recorded for temperatures in excess of 1700°C, with heating and cooling rates as high as 10,500°C  s−1 and 6500°C  s−1, respectively.

Place, publisher, year, edition, pages
2013. Vol. 30, no 7, 1835-1842 p.
Keyword [en]
Chemical composition gratings, Fiber diameters, Heating and cooling rates, Laser beam profiling, Spatial resolution, Thermal dynamics, Thermal response, Thermally stable
Keyword [sv]
Optiska fibrer Bragg gitter fiber sensor temperatur glas
National Category
Other Physics Topics
Identifiers
URN: urn:nbn:se:kth:diva-124330DOI: 10.1364/JOSAB.30.001835ISI: 000321337800007Scopus ID: 2-s2.0-84879987737OAI: oai:DiVA.org:kth-124330DiVA: diva2:634078
Funder
Swedish Research Council, 2007- 5533
Note

QC 20130703

Available from: 2013-06-28 Created: 2013-06-28 Last updated: 2017-12-06Bibliographically approved
In thesis
1. Laser processing of Silica based glass
Open this publication in new window or tab >>Laser processing of Silica based glass
2015 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

The main topic of this thesis work is photosensitivity and photo-structuring of optical fibers and bulk glass. Although research in the field of photosensitivity in glass and optical fibers has been ongoing for more than three decades, the underlying mechanisms are still not well understood. The objective was to gain a better understanding of the photo-response by studying photosensitivity from a thermodynamic perspective, as opposed to established research focusing on point defects and structural changes, and strain and stress in optical fibers. Optical fibers was mainly used for experimental studies for two reasons; first, photosensitivity in fibers is more pronounced and more elusive compared to its bulk counterpart, and secondly, fibers provide a simplified structure to study as they experimentally can be seen as one-dimensional.Initially, ablation experiments on bulk glass were performed using picosecond infrared pulses. With a design cross section of 40x40 μm, straight channels were fabricated on the top (facing incident light) and bottom side of the sample and the resulting geometries were analyzed. The results show a higher sensitivity to experimental parameters for bottom side ablation which was ascribed to material incubation effects. Moreover, on the top side, the resulting geometry has a V-shape, independent of experimental parameters, related to the numerical aperture of the focusing lens, which was ascribed to shadowing effects.After this work, the focus shifted towards optical fibers, UV-induced fiber Bragg gratings (FBGs) and thermal processing with conventional oven and with a CO2 laser as a source of radiant heat.First, a system for CO2 laser heating of optical fibers was constructed. For measuring the temperature of the processed fibers, a special type of FBG with high temperature stability, referred to as "Chemical Composition Grating" (CCG) was used. A thorough characterization and temperature calibration was performed and the results show the temperature dynamics with a temporal resolution of less than one millisecond. The temperature profile of the fiber and the laser beam intensity profile could be measured with a spatial resolution limited by the grating length and diameter of the fiber. Temperatures as high as ~ 1750 °C could be measured with corresponding heating and cooling rates of 10.500 K/s and 6.500 K/s.Subsequently, a thorough investigation of annealing and thermal regeneration of FBGs in standard telecommunication fibers was performed. The results show that thermal grating regeneration involves several mechanisms. For strong regeneration, an optimum annealing temperature near 900 C was found. Two different activation energies could be extracted from an Arrhenius of index modulation and Braggv iwavelength, having a crossing point also around 900 °C, indication a balance of two opposing mechanisms.Finally, the thermal dynamics and spectral evolution during formation of long period fiber gratings (LPGs) were investigated. The gratings were fabricated using the CO2 laser system by periodically grooving the fibers by thermal ablation. Transmission losses were reduced by carefully selecting the proper processing conditions. These parameters were identified by mapping groove depth and transmission loss to laser intensity and exposure time.

Abstract [sv]

Huvudtemana i denna avhandling är fotokänslighet och fotostrukturering av optiska fibrer och bulk glas. Trots att forskning inom fotokänslighet i glas och optiska fibrer har pågått under mer än tre decennier är de bakomliggande mekanismerna ännu inte klarlagda. Syftet var att få en bättre förståelse för fotoresponsen genom att studera fotokäsligheten ur ett termodynamiskt perspektiv, i motsats till etablerad forskning med fokus på punktdefekter och strukturförändringar, samt mekaniska spännings effekter i optiska fibrer. Optiska fibrer användes för flertalet av de experimentella studierna av två skäl; för det första är fotokänsligheten i fibrer större och dessutom vet man mindre om bakomliggande mekanismer jämfört med motsvarande bulk glas, och för det andra kan fibrer vara enklare att studera eftersom de experimentellt kan ses som en endimensionell struktur.Inledningsvis utfördes ablaherings experiment på bulk glas med en infraröd laser med pikosekund pulser. Raka kanaler med ett designtvärsnitt på 40x40 μm tillverkades på ovansidan (mot infallande ljus) och bottensidan av provet och de resulterande geometrierna analyserades. Resultaten visar en högre känslighet för variationer i experimentella parametrar vid ablahering på undersidan vilket kan förklaras av inkubations effekter i materialet. Dessutom är den resulterande geometrin på ovansidan V-formad, oavsett experimentella parametrar, vilket kunde relateras till den numeriska aperturen hos den fokuserande linsen, vilket förklaras av skuggningseffekter.Efter detta arbete flyttades fokus mot optiska fibrer, UV inducerade fiber Bragg gitter (FBG), och termisk bearbetning med konventionell ugn samt även med en CO2-laser som källa för strålningsvärme.Först konstruerades ett system för CO2-laservärmning av fibrer. För mätning av temperaturen hos bearbetade fibrer användes en speciell sorts FBG med hög temperaturstabilitet, kallade ”Chemical Composition Gratings” (CCG). En grundlig karaktärisering och temperaturkalibrering utfördes och temperaturdynamiken mättes med en tidsupplösning på under en millisekund. Temperaturprofilen i fibern, och laserns strålprofil, kunde mätas med en spatiell upplösning begränsad av gitterlängden och fiberns diameter. Temperaturer upp till ~1750 °C, vilket är högre än mjukpunktstemperaturen, kunde mätas med korresponderande uppvärmnings- och avsvalningshastighet på 10.500 K/s och 6.500 K/s.Därefter gjordes en omfattande undersökning av värmebearbetning och termisk regenerering av FBG:er i telekomfiber. Resultaten visar att termisk gitter-regenerering aktiveras av flera olika mekanismer. Värmebearbetning vid en temperatur omkring 900 °C resulterade i starka gitter efter en regenerering vid en temperatur på 1100 °C. Två olika aktiveringsenergier kunde extraheras från en Arrhenius plot avseende brytningsindexmodulation och Braggvåglängd, med en skärningspunkt tillika runt 900 °C, vilket indikerar en avvägning mellan två motverkande mekanismer vid denna temperatur.Slutligen undersöktes temperaturdynamiken och de spektrala egenskaperna under tillverkning av långperiodiga fibergitter (LPG). Gittren tillverkades med CO2-vi iilasersystemet genom att skapa en periodisk urgröpning medelst termisk ablahering. Transmissionsförluster kunde reduceras med noggrant valda processparametrar. Dessa parametrar identifierades genom mätningar av ablaherat djup och transmissionsförlust som funktion av laserintensitet och exponeringstid.

Place, publisher, year, edition, pages
Stockholm: KTH Royal Institute of Technology, 2015. 88 p.
Series
TRITA-FYS, ISSN 0280-316X ; 2015:72
Keyword
Fiber Bragg Gratings, photosensitivity, Glass, laser machining, optical fibers, fiber sensor
National Category
Atom and Molecular Physics and Optics
Research subject
Physics
Identifiers
urn:nbn:se:kth:diva-173929 (URN)978-91-7595-709-8 (ISBN)
Public defence
2015-10-14, FB 52, AlbaNova Universitetscentrum, Roslagstullsbacken 21, Stockholm, 13:00 (English)
Opponent
Supervisors
Note

QC 20150924

Available from: 2015-09-24 Created: 2015-09-23 Last updated: 2015-09-24Bibliographically approved

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