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The first peripherally masked thiol dendrimers: a facile and highly efficient functionalization strategy of polyester dendrimers via one-pot xanthate deprotection/thiol-acrylate Michael addition reactions
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Coating Technology.
KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Coating Technology.ORCID iD: 0000-0002-9200-8004
2014 (English)In: Chemical Communications, ISSN 1359-7345, E-ISSN 1364-548X, Vol. 50, no 50, 6574-6577 p.Article in journal (Refereed) Published
Abstract [en]

Introducing multiple reactive functional groups at the periphery of dendrimer materials presents considerable challenges if the functionality is able to self-react. An efficient and facile approach to introducing masked thiols at the surface of polyester dendrimers is presented. One-pot, deprotection/thiol-acrylate Michael addition from the xanthate-functional dendritic substrates (generation zero to two) has been achieved for the first time, with high efficiency demonstrated using three acrylates of varying chemistry and avoiding disulfide formation.

Place, publisher, year, edition, pages
2014. Vol. 50, no 50, 6574-6577 p.
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-147441DOI: 10.1039/c3cc49704fISI: 000336837900003Scopus ID: 2-s2.0-84901593993OAI: oai:DiVA.org:kth-147441DiVA: diva2:730281
Note

QC 20140627

Available from: 2014-06-27 Created: 2014-06-27 Last updated: 2017-12-05Bibliographically approved

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Malkoch, Michael

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