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Capillary Electrophoretic Determination of Fluoroquinolones in Bovine Milk Followed by Off-Line MALDI-TOF-MS Analysis
KTH, School of Chemical Science and Engineering (CHE), Chemistry, Applied Physical Chemistry. INQUISUR (UNS-CONICET), Argentina.
KTH, School of Chemical Science and Engineering (CHE), Chemistry, Applied Physical Chemistry.ORCID iD: 0000-0003-3548-217X
KTH, School of Chemical Science and Engineering (CHE), Chemistry, Applied Physical Chemistry.
INQUISUR (UNS-CONICET), Argentina.
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2015 (English)In: Chromatographia, ISSN 0009-5893, E-ISSN 1612-1112, Vol. 78, no 3-4, 285-290 p.Article in journal (Refereed) Published
Abstract [en]

A novel appro ach for the determination of ciprofloxacin, norfloxacin and ofloxacin by capillary electrophoresis and off-line capillary electrophoresis-matrix-assisted laser desorption/ionization-time of flight-mass spectrometry coupling for the confirmation of analyte identities is presented. A polymer capillary coating was proposed with the aim to minimize suppression of the MS signal caused by the CE solution components. The fluoroquinolones were successfully separated and determined by CE-UV followed by fractionation onto a MALDI plate and off-line MS characterization. Full-cream and low-fat milk samples were used to illustrate that the proposed method represents an efficient alternative for fluoroquinolone antibiotics determination in milk.

Place, publisher, year, edition, pages
2015. Vol. 78, no 3-4, 285-290 p.
Keyword [en]
Capillary electrophoresis, Matrix-assisted laser desorption/ionization mass spectrometry, Fluoroquinolones, Off-line integration
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:kth:diva-161110DOI: 10.1007/s10337-014-2823-5ISI: 000348976900016Scopus ID: 2-s2.0-84925487438OAI: oai:DiVA.org:kth-161110DiVA: diva2:797201
Note

QC 20150323

Available from: 2015-03-23 Created: 2015-03-09 Last updated: 2017-12-04Bibliographically approved

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Jacksén, JohanEmmer, Åsa

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