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  • 1.
    Leijonmarck, Simon
    et al.
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH).
    Carlson, T.
    Hellqvist Kjell, Maria
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH).
    Asp, L. E.
    Lindbergh, Göran
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemical Engineering, Applied Electrochemistry.
    Maples, H.
    Bismarck, A.
    Coated carbon fibre battery half-cells for structural battery composites2013In: ICCM International Conferences on Composite Materials, International Committee on Composite Materials , 2013, p. 5342-5343Conference paper (Refereed)
  • 2.
    Leijonmarck, Simon
    et al.
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH).
    Pupurs, A.
    Asp, L.
    Strength of thin solid polymer electrolyte coatings and the coated carbon fibres2015In: ICCM International Conferences on Composite Materials, International Committee on Composite Materials , 2015Conference paper (Refereed)
    Abstract [en]

    As a route to increase the efficiency of electric vehicles, weight reductions through composite building materials are constantly being introduced. To further aid this effort focus has been put on structural batteries, where the composite is multifunctional serving both as energy storing as well as load bearing unit. In an attempt to reduce the high ionic resistances solid polymer electrolytes introduces, carbon fibres have been individually coated with polymeric layers ranging from <500 nm to >3 µm in thickness. This study investigates the feasibility of using such coatings in structural applications with respect to mechanical load cycling. The coated fibres were subjected to cyclic load up to approximately 1 % strain for up to 70,000 cycles. The polymer coatings were found not to be visibly affected by the prolonged mechanical fatigue. No cracks were observed in the coatings which makes the coating technique promising for future structural battery applications. © 2015 International Committee on Composite Materials. All rights reserved.

  • 3.
    Lu, Huiran
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry.
    Behm, Mårten
    KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry.
    Leijonmarck, Simon
    KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry. Swerea KIMAB AB.
    Lindbergh, Göran
    KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry.
    Cornell, Ann M.
    KTH, School of Chemical Science and Engineering (CHE), Chemical Engineering and Technology, Applied Electrochemistry. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    Flexible Paper Electrodes for Li-Ion Batteries Using Low Amount of TEMPO-Oxidized Cellulose Nanofibrils as Binder2016In: ACS Applied Materials and Interfaces, ISSN 1944-8244, E-ISSN 1944-8252, Vol. 8, no 28, p. 18097-18106Article in journal (Refereed)
    Abstract [en]

    Flexible Li-ion batteries attract increasing interest for applications in bendable and wearable electronic devices. TEMPO-oxidized cellulose nanofibrils (TOCNF), a renewable material, is a promising candidate as binder for flexible Li-ion batteries with good mechanical properties. Paper batteries can be produced using a water-based paper making process, avoiding the use of toxic solvents. In this work, finely dispersed TOCNF was used and showed good binding properties at concentrations as low as 4 wt %. The TOCNF was characterized using atomic force microscopy and found to be well dispersed with fibrils of average widths of about 2.7 nm and lengths of approximately 0.1-1 mu m. Traces of moisture, trapped in the hygroscopic cellulose, is a concern when the material is used in Li-ion batteries. The low amount of binder reduces possible moisture and also increases the capacity of the electrodes, based on total weight. Effects of moisture on electrochemical battery performance were studied on electrodes dried at 110 degrees C in a vacuum for varying periods. It was found that increased drying time slightly increased the specific capacities of the LiFePO4 electrodes, whereas the capacities of the graphite electrodes decreased. The Coulombic efficiencies of the electrodes were not much affected by the varying drying times. Drying the electrodes for 1 h was enough to achieve good electrochemical performance. Addition of vinylene carbonate to the electrolyte had a positive effect on cycling for both graphite and LiFePO4. A failure mechanism observed at high TOCNF concentrations is the formation of compact films in the electrodes.

  • 4.
    Nowak, Andrzej
    et al.
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemical Engineering, Applied Electrochemistry.
    Hagberg, Johan
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemical Engineering.
    Leijonmarck, Simon
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemical Engineering.
    Schweinebarth, Hannah
    Baker, Darren
    Uhlin, Anders
    Tomani, Per
    Lindbergh, Göran
    KTH, School of Engineering Sciences in Chemistry, Biotechnology and Health (CBH), Chemical Engineering.
    Lignin-based carbon fibers for renewable and multifunctional lithium-ion battery electrodes2018In: Holzforschung, ISSN 0018-3830, E-ISSN 1437-434X, Vol. 72, no 2, p. 81-90Article in journal (Refereed)
    Abstract [en]

    Lignin-based carbon fibers (LCFs) from the renewable resource softwood kraft lignin were synthesized via oxidative thermostabilization of pure melt-spun lignin and carbonization at different temperatures from 1000 degrees C to 1700 degrees C. The resulting LCFs were characterized by tensile testing, scanning electron microscopy (SEM), X-ray diffraction (XRD) and confocal Raman spectroscopy. The microstructure is mainly amorphous carbon with some nanocrystalline domains. The strength and stiffness are inversely proportional to the carbonization temperature, while the LCFs carbonized at 1000 degrees C exhibit a strength of 628 MPa and a stiffness of 37 GPa. Furthermore, the application potential of LCFs was evaluated as negative electrodes in a lithium-ion battery (LIB) by electrochemical cycling at different current rates in a half-cell setup. The capacity drops with the carbonization temperature and the LCFs carbonized at 1000 degrees C have a capacity of 335 mAh g(-1). All LCFs showed good cycling stability. Because of the mechanical integrity and conductivity of the LCFs, there is no need to apply current collectors, conductive additives or binders. The advantage is an increased gravimetric energy density compared to graphite, which is the most common negative electrode material. LCFs show a promising multifunctional behavior, including good mechanical integrity, conductivity and an ability to intercalate lithium for LIBs.

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