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  • 1.
    Zhu, Hongli
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Areskogh, Dimitri
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Helander, Mikaela
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Henriksson, Gunnar
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    A preliminary investigation on enzymatic oxidative polymerization of lignin2011In: 16th International Symposium on Wood, Fiber and Pulping Chemistry: Proceedings, ISWFPC, 2011, p. 238-241Conference paper (Refereed)
    Abstract [en]

    Enzyme catalyzed oxidative polymerization of technical bagasse lignin and low-molecular-weight ultra-filtered kraft pulp lignin (UFL) were studied in methanol-water solution. Lignin was dissolved in methanol-water solution at pH 13 in steam heated autoclave at 130°C for 2h. The polymerization reaction was conducted at 40°C with a commercial laccase under oxygen saturation. The weight-average molecular weight (Mw) of original macromonomer and polymerized lignin were characterized with alkaline size exclusion Chromatograph (SEC) system. Enzyme treatment increased the molecular weight of both technical bagasse lignin and ultra-filtered lignin up to 20 times. The reaction time and the enzyme dosage were studied to obtain the maximal molecular weight.

  • 2.
    Zhu, Hongli
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Areskogh, Dimitri
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Helander, Mikaela
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Henriksson, Gunnar
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Investigation on enzymatic oxidative polymerization of technical soda lignin2012In: Abstract of Papers of the American Chemical Society, ISSN 0065-7727, Vol. 243Article in journal (Other academic)
  • 3.
    Zhu, Hongli
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Areskogh, Dimitri
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Helander, Mikaela
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    Henriksson, Gunnar
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    Investigation on enzymatic oxidative polymerization of technical soda lignin2012In: Current organic chemistry, ISSN 1385-2728, E-ISSN 1875-5348, Vol. 16, no 16, p. 1850-1854Article in journal (Refereed)
    Abstract [en]

    Enzyme, including laccase and peroxidase, catalyzed oxidative polymerization of technical bagasse soda lignin and low molecular weight ultra-filtrated kraft pulp lignin in methanol-water solution were studied. The weight average molecular weight of original macromonomer and polymerized lignin were characterized with alkaline size exclusion chromatograph system. Laccase treatment increased the molecular weight of both technical bagasse lignin and ultra-filtrated lignin up to 20 times in 24h. Compared to the low molecular weight ultra filtrated lignin, the reaction rate of bagasse lignin was consistant during the whole procedure. The reaction time and the laccase dosage were investigated to obtain the maximal molecular weight. The horseradish peroxidase treatment was a potential method for low molecular weight ultra filtrated lignin.

  • 4.
    Zhu, Hongli
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Helander, Mikaela
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    Moser, Carl
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
    Ståhlkranz, Adam
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
    Söderberg, Daniel
    KTH, School of Engineering Sciences (SCI), Mechanics.
    Henriksson, Gunnar
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    Lindström, Mikael
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology. KTH, School of Chemical Science and Engineering (CHE), Centres, Wallenberg Wood Science Center.
    A novel nano cellulose preparation method and size fraction by cross flow ultra- filtration2012In: Current organic chemistry, ISSN 1385-2728, E-ISSN 1875-5348, Vol. 16, no 16, p. 1871-1875Article in journal (Refereed)
    Abstract [en]

    A novel energy-efficient method called nanopulping (patent pending) to produce nanocellulose from chemical pulp, and a novel cross-flow ultra-filtration method to separate nanofibrils fractions of different size were applied in this study. Pretreatment with endoglucanase or 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) oxidation seems to enhance the nanopulping process. Results were evaluated with atomic force microscope and ultrafiltration. The nanopulping produced a relatively inhomogeneous material with larger particles/ fibers in addition to nanofibers. However, by ultrafiltration of the material it was possible to obtain more homogeneous material in different dimensions with methods industrially acceptable.

  • 5.
    Zhu, Hongli
    et al.
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology.
    Li, Yuanyuan
    Pettersson, Bert
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Fibre Technology.
    Zhang, Liming
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Lindström, Mikael
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Henriksson, Gunnar
    KTH, School of Chemical Science and Engineering (CHE), Fibre and Polymer Technology, Wood Chemistry and Pulp Technology.
    Technical soda lignin dissolved in urea as an environmental friendly binder in wood fiberboard2014In: Journal of Adhesion Science and Technology, ISSN 0169-4243, E-ISSN 1568-5616, Vol. 28, no 5, p. 490-498Article in journal (Refereed)
    Abstract [en]

    The application of lignin as binder in wood composite panel is not only environmentally friendly but also commercially attractive. The dissolving of technical soda lignin is the most premier challenge in its application. In this study, the effect of different key factors on soda lignin solubility in urea was investigated. The maximum solubility of 60.16g/L was obtained under the temperature 70 degrees C, urea concentration 8M, lignin content 7%, and pH 8.8. Then, different kinds of wood fiber material were mixed with the dissolved lignin solution to make fiber board separately. The results showed that the lignin can enhance the tensile strength of particleboard and can be used as a binder in wood material, but the strength will be different with different materials. The optimal tensile strength obtained was 44.63MPa with the sample made from oriented cotton linter sheet.

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