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Rashid, Masud-Ur
Publications (6 of 6) Show all publications
Rashid, M.-U., Tomkowski, R. & Archenti, A. (2025). Extending tool life: High-dynamic stiffness nanocomposite coating for improved machining performance. Surface & Coatings Technology, 515, Article ID 132604.
Open this publication in new window or tab >>Extending tool life: High-dynamic stiffness nanocomposite coating for improved machining performance
2025 (English)In: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 515, article id 132604Article in journal (Refereed) Published
Abstract [en]

Numerous studies are available regarding the effect of PVD and CVD coatings on cutting tools (inserts), cutting parameter optimization, and the application of the minimum quantity lubrication on the reduction of cutting tool wear and the improvement in surface quality of the machined parts. However, there still exists the deficiency of the comprehensive analysis of improving machining performance by suppressing high frequency vibration (micro-vibration) at the cutting edge due to the random nature of cutting force. The present study aims to mitigate this challenge of suppressing micro-vibration by applying the high dynamic stiffness multilayered Cu: CuCN<inf>x</inf> nanocomposite coating at the close proximity of cutting edge (in between the cutting insert and shim) by synthesizing the Cu:CuCN<inf>x</inf> coating on conventional cemented carbide (WC-Co) square shims. The primary objective of this study was to experimentally investigate the effect of Cu:CuCN<inf>x</inf> coating's morphology on machining performance. Coating morphology was characterized by the total coating thickness and total number of alternative Cu and CuCN<inf>x</inf> layers in a certain coating thickness. Machining performance was evaluated based on the criteria of cutting tool life and machined part's surface quality. External longitudinal turning operations of SS2541-03 alloy steel (34CrNiMoS6) material with rough cutting parameters and wet condition (using cutting fluid) were adopted for evaluating machining performance. Three different Cu:CuCN<inf>x</inf> coating series- A, B and C were synthesized by means of a double cathode Reactive High-Power Impulse Magnetron Sputtering (R-HiPIMS) deposition system. Coatings of series-A were deposited on steel disc substrates, and were used to evaluate the Cu:CuCN<inf>x</inf> nanocomposite coating's mechanical properties as a function of total number of Cu and CuCN<inf>x</inf> layers in a fixed coating thickness. Mechanical properties of the coatings were investigated by Vickers micro-indentation, and the damping loss factor of the coating was evaluated on the basis of indentation creep measurements under room temperature. Results from the analysis with coating series A demonstrated that the maximum elastic modulus, loss factor and loss modulus values of the coating was obtained when the ratio of total number Cu and CuCN<inf>x</inf> layers to coating thickness (n/h) is 0.6. However, the hardness, H/E and H<sup>3</sup>/E<sup>2</sup> values were observed to be increasing with increasing number of total layers. The coating with optimum mechanical properties exhibited the highest loss modulus of 2.85 ± 0.03 GPa confirming the high dynamic stiffness of Cu:CuCN<inf>x</inf> nanocomposite. Coated shims prepared with coating series- B and C were used to evaluate the effect of total number of Cu and CuCN<inf>x</inf> layers and the effect of total coating thickness on the machining performance, respectively. From the turning tests with conventional shim and coated shims it was evident that the coated shim with 200 μm Cu:CuCN<inf>x</inf> coating (sample C3) increased the cutting tool life by at least 50 % and reduced the machined workpiece's surface roughness by 15 %. For all turning tests, the thicknesses of coated shims and corresponding conventional uncoated shim were kept constant. The maximum error between the experimental and predicted values of the mechanical properties of coating series-B was found to be less than 10 %Moreover, in case of 200 μm Cu:CuCN<inf>x</inf> coating containing 150 layers of Cu and CuCN<inf>x</inf> phases, the coated shim (sample B3) was able to increase the cutting tool life by at least 167 %, and the machined workpiece's average surface roughness was reduced by 10 %. Analysis of the acquired vibration signals during turning tests, indicated that the cutting tool life was prominently affected by the higher frequency vibration (>7000 Hz) at the tool's cutting-edges. It was observed that with the application of 200 μm Cu:CuCN<inf>x</inf> coating in coated shim, the root mean squared (RMS) vibration energy in overall frequency range (0 to 30,000 Hz) was reduced by 40 %. From material and mechanical characterization, it was postulated that the primary vibration energy dissipation mechanisms of the multilayered nanocomposite coating are the interface frictional energy loss between the alternative Cu and CuCN<inf>x</inf> layers and the intrinsic damping due to grain boundary sliding in CuCN<inf>x</inf> layers.

Place, publisher, year, edition, pages
Elsevier BV, 2025
Keywords
Alloy steel, Cu:CuCNx nanocomposite, Cutting tool life, Damping loss factor, Dynamic stiffness, High frequency vibration, HiPIMS, Loss modulus, Machining performance, Metal matrix composite (MMC), Multilayer coating, Surface roughness, Tool wear, Turning
National Category
Manufacturing, Surface and Joining Technology
Identifiers
urn:nbn:se:kth:diva-369848 (URN)10.1016/j.surfcoat.2025.132604 (DOI)001564052900001 ()2-s2.0-105014289846 (Scopus ID)
Note

QC 20250917

Available from: 2025-09-17 Created: 2025-09-17 Last updated: 2025-09-17Bibliographically approved
Rashid, M.-U., Tomkowski, R. & Archenti, A. (2022). Effect of Surface Pre-Treatment on the Adhesion between HiPIMS Thick Cu:CuCNx Coating and WC-Co Shim. Coatings, 12(10), Article ID 1484.
Open this publication in new window or tab >>Effect of Surface Pre-Treatment on the Adhesion between HiPIMS Thick Cu:CuCNx Coating and WC-Co Shim
2022 (English)In: Coatings, ISSN 2079-6412, Vol. 12, no 10, article id 1484Article in journal (Refereed) Published
Abstract [en]

High-power impulse magnetron-sputtering thick metal/carbon-nitride-doped metal-matrix multilayer nano-composite coating can be applied to cutting-tool holder components to improve cutting insert's life. One of the challenges of such an add-on solution is the poor adhesion between the thick coating and the hard alloy substrate, such as WC-Co shim. This work presents a study on WC-Co substrate surface preparation methods for HiPIMS coating and its adhesion improvement. Three mechanical surface pretreatment methods were investigated: machining (grinding), diamond polishing, and grit blasting. White-light interferometry was used for substrate surface texture measurement before and after pretreatment. It was demonstrated that, compared to machining and diamond polishing, grit blasting can significantly improve the interface adhesion between the similar to 200 mu m-thick Cu:CuCNx coating and WC-Co shim. Grit blasting was also found to be beneficial for improving the cutting insert's life in the external turning process. In turning tests, the coating lifetime for grit-blasted shim was more than 90 min, whereas the coating lifetimes for machined shim (conventional shim) and diamond-polished shim were similar to 85 min and similar to 70 min, respectively. Further, by comparing the HiPIMS gradient chromium pre-layer between the coating and substrate for the different shims, the study also explained that the quasi-isotropic surface texture of grit-blasted shim is more advantageous for coating-substrate interface adhesion.

Place, publisher, year, edition, pages
MDPI, 2022
Keywords
surface texture, pre-treatment, grit blasting, HiPIMS, Cu:CuCNx thick coatings, adhesion, nano-composite, WC-Co shim, insert wear, turning
National Category
Manufacturing, Surface and Joining Technology
Identifiers
urn:nbn:se:kth:diva-321263 (URN)10.3390/coatings12101484 (DOI)000872407300001 ()2-s2.0-85140885761 (Scopus ID)
Note

QC 20221114

Available from: 2022-11-14 Created: 2022-11-14 Last updated: 2025-03-28Bibliographically approved
Shakir, M., Hou, S., Metreveli, A., Rashid, M.-U., Mantooth, H. A. & Zetterling, C.-M. (2019). 555-Timer IC Operational at 500 °C.
Open this publication in new window or tab >>555-Timer IC Operational at 500 °C
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2019 (English)Manuscript (preprint) (Other academic) [Artistic work]
Abstract [en]

This paper reports an industry standard monolithic 555-timer circuit designed and fabricated in the in-house silicon carbide (SiC) low-voltage bipolar technology. The paper demonstrates the 555-timer ICs characterization in both astable and monostable modes of operation, with a supply voltage of 15 V over the wide temperature range of 25 to 500°C. Nonmonotonictemperature dependence was observed for the 555-timer IC frequency, rise-time, fall-time, and power dissipation.

National Category
Engineering and Technology
Identifiers
urn:nbn:se:kth:diva-251765 (URN)
Funder
Knut and Alice Wallenberg Foundation
Note

QC 20190523

Available from: 2019-05-21 Created: 2019-05-21 Last updated: 2022-06-26Bibliographically approved
rashid, M.-U. a. & Archenti, A. (2018). Manufacturing and Characterization of a Carbon-Based Amorphous (a-CNX) Coating Material. Nanomanufacturing and Metrology, 1(1), 1-14
Open this publication in new window or tab >>Manufacturing and Characterization of a Carbon-Based Amorphous (a-CNX) Coating Material
2018 (English)In: Nanomanufacturing and Metrology, ISSN 2520-8128, Vol. 1, no 1, p. 1-14Article in journal (Refereed) Published
Abstract [en]

A thick 400-micron amorphous carbon nitride (a-CNX ) coating material was synthesized by means of plasma-enhanced chemical vapor deposition process. High-power impulse magnetron sputtering technique was used to sputter a pure graphite target plate in reactive argon (Ar), nitrogen (N2 ) and acetylene (C2 H2 ) environment for depositing the omposite coating. Structural and chemical/elemental composition of the a-CNX  composite material was investigated by field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy and micro-Raman spectroscopy. The rootmean-square surface roughness (Sq ) and structure were estimated by atomic force microscopy. Mechanical properties such as hardness and Young’s modulus (Oliver–Pharr method) at room temperature were characterized by Vickers microindentation test. Operational temperature test of the deposited a-CNX  coating reveals that it can withstand up to 400 C without cracking. An inverted shaker test, based on central impedance method, was adopted to investigate the dynamic damping property of the coating material, and it was found that the first bending mode damping lossfactor of the reported a-CNX  coating is 0.015 ±  0.001 and corresponding loss modulus (Young’s modulus multiplied by lossfactor) is 0.234 ±  0.011 GPa.

Place, publisher, year, edition, pages
Singapore: Springer, 2018
Keywords
PECVD, Reactive HiPIMS, Amorphous carbon nitride (a-CNx), Mechanical properties, Material properties, System damping lossfactor, Material damping lossfactor
National Category
Production Engineering, Human Work Science and Ergonomics
Research subject
Production Engineering
Identifiers
urn:nbn:se:kth:diva-231981 (URN)10.1007/s41871-018-0014-y (DOI)2-s2.0-85083490691 (Scopus ID)
Funder
XPRES - Initiative for excellence in production research
Note

QC 20180808

Available from: 2018-07-06 Created: 2018-07-06 Last updated: 2024-03-15Bibliographically approved
Fu, Q., Rashid, M.-U. M., Nicolescu, C.-M., Toth, G. & et al., . (2016). High dynamic stiffness mechanical structures with nanostructured composite coatings deposited by high power impulse magnetron sputtering. Carbon, 98, 24-33
Open this publication in new window or tab >>High dynamic stiffness mechanical structures with nanostructured composite coatings deposited by high power impulse magnetron sputtering
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2016 (English)In: Carbon, ISSN 0008-6223, E-ISSN 1873-3891, Vol. 98, p. 24-33Article in journal (Refereed) Published
Abstract [en]

Nanostructured Cu:CuCNx composite coatings with high static and dynamic stiffness were synthesized by means of plasma-enhanced chemical vapor deposition (PECVD) combined with high power impulse magnetron sputtering (HiPIMS). Scanning electron microscope (SEM) images and energy-dispersive X-ray spectroscopy (EDS) mapping from cross-sectioned samples reveals a multi-layered nanostructure enriched in Cu, C, N, and O in different ratios. Mechanical properties of the coatings were investigated by Vickers micro-indention and model tests. It was observed that copper inclusions as well as copper interlayers in the CNx matrix can increase mechanical damping by up to 160%. Mechanical properties such as hardness, elastic modulus and loss factor were significantly improved by increasing the discharge power of the sputtering process. Moreover the coatings loss modulus was evaluated on the basis of indentation creep measurements under room temperature. The coating with optimum properties exhibited loss modulus of 2.6 GPa. The composite with the highest damping loss modulus were applied on the clamping region of a milling machining tool to verify their effect in suppressing regenerative tool chatter. The high dynamic stiffness coatings were found to effectively improve the critical stability limit of a milling tool by at least 300%, suggesting a significant increase of the dynamic stiffness.

Place, publisher, year, edition, pages
Elsevier, 2016
National Category
Composite Science and Engineering Production Engineering, Human Work Science and Ergonomics Applied Mechanics Nano Technology Other Physics Topics
Research subject
Materials Science and Engineering; Production Engineering; Solid Mechanics; Chemistry
Identifiers
urn:nbn:se:kth:diva-176864 (URN)10.1016/j.carbon.2015.10.074 (DOI)000367233000003 ()2-s2.0-84955307996 (Scopus ID)
Projects
HiPPOCAMP
Funder
EU, FP7, Seventh Framework Programme, 608800
Note

QC 20160209

Available from: 2015-11-10 Created: 2015-11-10 Last updated: 2024-03-15Bibliographically approved
Frangoudis, C., Fu, Q., Ur Rashid, M. M. M., Nicolescu, C. M. & Rashid, A. (2013). Experimental analysis of the CNx nano-damping material’s effect on the dynamic performance of a milling process. In: Archenti, Andreas; Maffei, Antonio (Ed.), Proceedings of the International Conference on Advanced Manufacturing Engineering and Technologies: . Paper presented at Proceedings of the International Conference on Advanced Manufacturing Engineering and Technologies NEWTECH 2013; Stockholm, Sweden, 27-30 October, 2013 (pp. 293-302). Stockholm: KTH Royal Institute of Technology
Open this publication in new window or tab >>Experimental analysis of the CNx nano-damping material’s effect on the dynamic performance of a milling process
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2013 (English)In: Proceedings of the International Conference on Advanced Manufacturing Engineering and Technologies / [ed] Archenti, Andreas; Maffei, Antonio, Stockholm: KTH Royal Institute of Technology, 2013, p. 293-302Conference paper, Published paper (Refereed)
Abstract [en]

Vibration phenomena are a main consideration during the material removal operation, as it has prominent effects on the product quality, cutting tool life, and productivity of that machining operation. Within the context of machining performance, role of enhanced stiffness and damping on the dynamic behaviour of machining systems such as turning and milling is well established. In this experimental analysis, investigations have been conducted for identifying the natural characteristics and dynamic responses of a milling process with the application of a novel carbon based (CNx) nano-composite damping material. TheCNx material has been applied into the joint interface of a workholding device with adaptive dynamic stiffness. Prior investigations of this material, produced by theplasma enhanced chemical vapor (PECVD) process, showed inherent damping capacity via interfacial frictional losses of its micro-columnar structures. For thisstudy, natural characteristics of the workholding system have been characterized bythe modal impact testing method. Dynamic responses during the machining processhave been measured through the vibration acceleration signals. The ultimate objective of this study is to comprehend the potentiality of CNx coating material forimproving machining process performance by analyzing the frequency response functions and measured vibration signals of the investigated milling process with varying stiffness and damping levels.

Place, publisher, year, edition, pages
Stockholm: KTH Royal Institute of Technology, 2013
Keywords
carbon based nano-composite material
National Category
Production Engineering, Human Work Science and Ergonomics
Research subject
SRA - Production
Identifiers
urn:nbn:se:kth:diva-140737 (URN)978-91-7501-892-8 (ISBN)
Conference
Proceedings of the International Conference on Advanced Manufacturing Engineering and Technologies NEWTECH 2013; Stockholm, Sweden, 27-30 October, 2013
Projects
EU FP7 PoPJIM
Funder
XPRES - Initiative for excellence in production research
Note

QC 20140205

Available from: 2014-01-31 Created: 2014-01-31 Last updated: 2024-03-15Bibliographically approved
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