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On the quantification of healing in asphalt materials
KTH, School of Architecture and the Built Environment (ABE), Civil and Architectural Engineering, Structural Engineering and Bridges.ORCID iD: 0000-0002-9013-1340
2021 (English)Licentiate thesis, comprehensive summary (Other academic)
Abstract [en]

Asphalt materials exhibit self-healing characteristics. In order to evaluate the healing capabilities of these materials, numerous investigations are carried out by researchers. These investigations include various definitions of healing and mechanical test methods to quantify the extent of healing. Irrespective of these extensive studies, there is no unique method to evaluate the healing in asphalt materials. The biasedness to the test conditions and complexity due to the involvement of other phenomena such as stress relaxation and strain recovery make the characterization of healing a challenging process. The work presented in this thesis includes the development of experimental and analytical approaches to contribute to the understanding of healing in asphalt materials. The thesis focuses on both fracture mechanics and damage mechanics-based approaches to evaluate the healing in asphalt materials. In the first case, three-point bending tests are carried out to characterize the healing following the fracture. The experimental protocol is carefully designed to avoid the effect due to low temperature physical hardening of the material during the rest period. Different healing indices appealing to linear elastic fracture mechanics and viscoelastic fracture mechanics are compared. While healing is generally defined based on the recovery of certain parameters following the rest period, the comparison across healing indices shows that the quantitative interpretations of healing are dependent on the post-processing methods. The damage mechanics-based approach discussed in this study includes creep and recovery tests in shear. Here, unlike the first case, the samples are not fractured during the test. The damage is considered to be a part of the viscoplastic deformation and the recovery of viscoplastic deformation is defined as the healing. The method proposed in this study is useful to isolate the viscoelastic effects to quantify the healing of damage. 

Abstract [sv]

Asfaltmaterial uppvisar självläkande egenskaper. För att utvärdera dess läkande förmågor utförs många undersökningar av forskare. Dessa undersökningar inkluderar olika definitioner av läkning och mekaniska testmetoder för att kvantifiera graden av läkningen. Trots dessa omfattande studier finns det ingen unik metod för att utvärdera läkning i asfaltsmaterial. Påverkan av testförhållandena och komplexiteten från inverkan av andra fenomen, såsom spänningsrelaxation och töjningsåterhämtning, gör karakteriseringen av läkning en utmanande process. Arbetet som presenteras i denna uppsats inkluderar utvecklingen av experimentella och analytiska metoder för att bidra till förståelsen av läkning i asfaltsmaterial. Uppsatsen fokuserar på både brottmekaniks- och skademekaniksbaserade metoder för att utvärdera läkning i asfaltsmaterial. I det första fallet utförs trepunktsböjningstest för att karakterisera läkningen efter brott. Det experimentella protokollet är noggrant designat för att undvika effekten av hårdnande vid låg temperatur under viloperioden. Dessutom jämförs olika läkningsindex baserade på linjärelastisk brottmekanik och viskoelastisk brottmekanik. Trots att läkning generellt definieras baserat på återhämtningen av vissa parametrar efter viloperioden, så visar jämförelsen av läkningsindexen att den kvantitativa tolkningen av läkning beror på metoderna för efterbehandling.  Den skademekaniksbaserade metoden som diskuteras i denna studie inkluderar kryp- och återhämtningstest i skjuvning. Till skillnad mot det första fallet så spricker här inte proven. Skadan anses istället vara del av den viskoplastiska deformationen och återhämtningen av viskoplastisk deformation är definierad som läkning. Metoden som föreslås i denna studie är användbar för att isolera de viskoelastiska effekterna för att kvantifiera läkningen av skada. 

Place, publisher, year, edition, pages
Stockholm, Sweden: KTH Royal Institute of Technology, 2021. , p. 57
Series
TRITA-ABE-DLT ; 2122
Keywords [en]
Healing, bitumen, mastic, viscoelastic strain, viscoplastic strain, fracture, creep and recovery
Keywords [sv]
Läkning, bitumen, mastic, viskoelastisk töjning, viskoplastisk töjning, brott, kryp and återhämtning
National Category
Civil Engineering Infrastructure Engineering Applied Mechanics
Research subject
Civil and Architectural Engineering, Structural Engineering and Bridges
Identifiers
URN: urn:nbn:se:kth:diva-295468ISBN: 978-91-7873-877-9 (print)OAI: oai:DiVA.org:kth-295468DiVA, id: diva2:1556266
Presentation
2021-06-11, Videolänk: https://kth-se.zoom.us/j/63628715307, Du som saknar dator /datorvana kontakta nicole.kringos@abe.kth.se / Use the e-mail address if you need technical assistance, Stockholm, 09:00 (English)
Opponent
Supervisors
Available from: 2021-05-21 Created: 2021-05-20 Last updated: 2022-06-25Bibliographically approved
List of papers
1. A state-of-the-art review on self-healing in asphalt materials: Mechanical testing and analysis approaches
Open this publication in new window or tab >>A state-of-the-art review on self-healing in asphalt materials: Mechanical testing and analysis approaches
2021 (English)In: Article in journal (Other academic) Submitted
Abstract [en]

Asphalt materials exhibit intrinsic healing capabilities. Researchers have carried out numerous investigations to characterize various aspects related to healing in asphalt materials since 1960s. Nevertheless, due to the complexity associated with the healing mechanism, a diverse and sometimes contradicting understanding in terms of experimental methods, models and numerical analysis exists. This paper attempts to give an overview of various asphalt healing studies with an emphasis on mechanical testing and analysis, and compares theories on the healing mechanism and their reported dependence on wide variety of factors including rest periods, temperature, aging, and moisture on the healing process. Bitumen, mastic, and asphaltic mixture levels are hereby included and the differences in the defined healing indices are discussed. The review shows that many of the commonly used analysis approaches can be challenged due to the co-existence of different phenomena during fatigue and healing. Possible post-processing methods that consider the non-linearity of the material response and decomposition of various modes of energy dissipation at multiple scales hold promise for unbiased quantification of healing.

Keywords
Self-healing, Healing mechanism, Mechanical tests, Healing index, Asphalt, Fatigue, Fracture
National Category
Civil Engineering Infrastructure Engineering
Research subject
Civil and Architectural Engineering
Identifiers
urn:nbn:se:kth:diva-295460 (URN)
Note

QC 20210527

Available from: 2021-05-20 Created: 2021-05-20 Last updated: 2024-03-15Bibliographically approved
2. On Indices Based Healing Quantification for Bituminous Materials
Open this publication in new window or tab >>On Indices Based Healing Quantification for Bituminous Materials
(English)In: Journal of materials in civil engineering, ISSN 0899-1561, E-ISSN 1943-5533Article in journal (Refereed) In press
Abstract [en]

In the present study, three-point bending tests are carried out using single-edge notched beam specimens of bitumen and mastic to quantify healing. Experiments are conducted at a controlled displacement rate of 1 mm per minute at -15 ℃. After the crack propagation, samples are given a rest period of 2 hours at 10 ℃ to promote healing before re-testing them. Two different analysis approaches appealing to linear elastic fracture mechanics and viscoelastic fracture mechanics are compared. In order to perform analysis based on viscoelastic fracture mechanics, the elastic-viscoelastic correspondence principle is used. The amount of healing after the rest period is quantified using various healing indices based on the recovery of stiffness, peak load, fracture toughness, fracture energy, and J-integral. From the analysis performed on bitumen and mastic samples, the study illustrates that the quantum of healing is different when comparing different healing indices. While the stiffness-based healing index demonstrated the healing ability of bitumen, other healing indices used in the study confirmed the higher healing potential of mastic. The healing based on critical value of J-integral shows a distinct difference in the healing of bitumen and mastic. The study emphasizes that the quantification of healing capacity when using different healing indices should be closely linked to its measured conditions.

Keywords
healing, fracture mechanics, three-point bending, healing indices, energy dissipation, stiffness, J-integral, bitumen, mastic.
National Category
Civil Engineering Applied Mechanics
Research subject
Civil and Architectural Engineering
Identifiers
urn:nbn:se:kth:diva-295466 (URN)
Note

QC 20210611

Available from: 2021-05-20 Created: 2021-05-20 Last updated: 2022-06-25Bibliographically approved
3. A new approach to quantify healing using creep and recovery: application to bituminous binders and mastic
Open this publication in new window or tab >>A new approach to quantify healing using creep and recovery: application to bituminous binders and mastic
(English)In: Article in journal (Refereed) Submitted
Abstract [en]

The definition and quantification of healing of bituminous materials is a complex process that has given rise to a wide range of publications on healing test methods and post-processing procedures. The main issue in such investigations is that most of them still include the recovery due to the viscoelasticity of material into its healing potential. In this study, a new approach is used to quantify the healing devoid of viscoelastic recovery. The method is based on the assumption that the total strain in the material additively decomposes into viscoelastic and viscoplastic strains. The present study defines healing as the recovery of the quantum of viscoplastic strain. Creep and recovery experiments are carried out on bitumen and mastic at a wide range of stress levels at 5 and 15 ◦C. A 70/100 penetration grade bitumen and silica-based filler passing 75 µm sieve are used.The proposed method is applied to these experimental data sets to separate the viscoelastic and viscoplastic strains from the total strain. The healing measure used in this study considers the change in viscoplastic strain during the recovery period to the maximum value of viscoplastic strain generated during the creep. At any stress levels, the extent of viscoplastic strain and recovery is found to be considerably different between binder and mastic. The maximum values of viscoplastic deformation observed for bitumen and mastic are 31.7 and 6.2 %, respectively. The corresponding healing measures at the end of recovery period are 15.8 and 21.7 % for bitumen and mastic, respectively. At both test temperatures, the amount of healing is found to increase with the decrease in stress levels for both bitumen and mastic. Future work will focus on the separation of damage from the viscoplastic strain to validate a constitutive model that is able to simulate the damage and healing process.

Keywords
Healing, Viscoelasticity, Viscoplasticity, Bitumen, Mastic, Creep, Recovery
National Category
Civil Engineering Infrastructure Engineering
Research subject
Civil and Architectural Engineering
Identifiers
urn:nbn:se:kth:diva-295467 (URN)
Note

QC 20210609

Available from: 2021-05-20 Created: 2021-05-20 Last updated: 2022-06-25Bibliographically approved

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Varma, Remya

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