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Temperature measurements on silicon core fibers during CO2 laser processing
KTH, School of Engineering Sciences (SCI), Applied Physics, Laser Physics.ORCID iD: 0000-0002-7406-968X
2022 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

This thesis presents temperature measurements on silicon core optical fibers during CO2 laser processing. Silicon core fibers are a new type of fiber offering a unique platform to combine the optoelectronic properties of silicon and the possibilities of the optical fiber platform. This makes them a promising candidate for many applications, such as mid-IR detection and transmission, studies of nonlinear optical devices, or fiber amplifiers. Today, two hurdles limit their usage: high optical transmission losses and complicated coupling into the core due to its high refractive index. The first task of this thesis work was to find suitable postprocessing of the as-drawn fibers in order to decrease optical transmission losses. The goal was to improve the fibers by the liquid-phase recrystalliza[1]tion method. In this method, the core of the fiber is heated to a temperature above its melting point by a laser beam. By scanning the beam along the fiber, a melt zone is moved through the fiber. When the silicon solidifies, it recrystallizes into a single crystal with lower optical losses. Successively, a fully computer-controlled setup was developed for fiber processing. Furthermore, a lab-size fiber draw tower was built to fabricate specialty fibers, especially silicon core fibers. Here, a CO laser acts as the heat source. The developed draw tower is very flexible and can be used to manufacture ample amounts of many fiber types quickly. It is known that the cooling rate at which the silicon core solidifies is a crucial parameter for the final transmission losses. Yet, it has so far only been estimated from black-body radiation. Here, an interferometric method was developed, allowing for in-situ temperature measurements in silicon core optical fibers. The method relies on probing the fiber with a laser beam during processing and observing the interference pattern caused by glass reflections. A suitable calibration of the interference pattern with temperature allowed to remotely monitor the fiber temperature in real-time during processing with high precision.

Place, publisher, year, edition, pages
Stockholm: KTH Royal Institute of Technology, 2022. , p. 116
Series
TRITA-SCI-FOU ; 2021:54
National Category
Other Physics Topics
Research subject
Physics
Identifiers
URN: urn:nbn:se:kth:diva-307103ISBN: 978-91-8040-110-4 (print)OAI: oai:DiVA.org:kth-307103DiVA, id: diva2:1626486
Public defence
2022-02-04, Sal FA31 https://kth-se.zoom.us/j/64869625354, Roslagstullsbacken 21, Fysikcentrum, Albanova, Stockholm, 13:00 (English)
Opponent
Supervisors
Available from: 2022-01-11 Created: 2022-01-11 Last updated: 2022-06-25Bibliographically approved
List of papers
1. In-situ non-contact high-temperature measurement of an optical fiber up to the glass softening point
Open this publication in new window or tab >>In-situ non-contact high-temperature measurement of an optical fiber up to the glass softening point
2021 (English)In: Optics Express, E-ISSN 1094-4087, Vol. 29, no 5, p. 7825-7832Article in journal (Refereed) Published
Abstract [en]

The optical fiber itself can function as a partially reflecting concentric cavity interferometer when transversely probed by a focused laser beam. In this study, the thermal response of the fiber heated by a CO2-laser beam was characterized by monitoring the back-scattered interference pattern. Simultaneous measurement of the Bragg wavelength shift of an inscribed, high-temperature stable fiber Bragg grating allowed for calibration of the temperature-dependent phase response of the interferometer. The presented technique allows for in-situ non-contact temperature measurements up to the glass softening point.

Place, publisher, year, edition, pages
OPTICAL SOC AMER, 2021
National Category
Atom and Molecular Physics and Optics Other Physics Topics
Identifiers
urn:nbn:se:kth:diva-292479 (URN)10.1364/OE.417175 (DOI)000624968100123 ()33726276 (PubMedID)2-s2.0-85101838894 (Scopus ID)
Note

QC 20210412

Available from: 2021-04-12 Created: 2021-04-12 Last updated: 2022-09-15Bibliographically approved
2. High-performance arduino-based interferometric quadrature phase-shift detection system with 1 nm resolution
Open this publication in new window or tab >>High-performance arduino-based interferometric quadrature phase-shift detection system with 1 nm resolution
2021 (English)In: AIP Advances, E-ISSN 2158-3226, Vol. 11, no 10, p. 105304-, article id 105304Article in journal (Refereed) Published
Abstract [en]

A quadrature phase-shift detection system for interferometry has been conceptualized and evaluated. The main components, a microcontroller and two photodetectors, make a versatile low-cost detection system for displacement measurements or more generally phase-change measurements. The system is capable of sampling at 5 kHz with a spatial resolution of 1 nm.& nbsp;

Place, publisher, year, edition, pages
AIP Publishing, 2021
National Category
Telecommunications Atom and Molecular Physics and Optics
Identifiers
urn:nbn:se:kth:diva-305531 (URN)10.1063/5.0055484 (DOI)000721712000005 ()2-s2.0-85117081844 (Scopus ID)
Note

QC 20211215

Available from: 2021-12-15 Created: 2021-12-15 Last updated: 2023-03-28Bibliographically approved
3. Specialty optical fiber fabrication: fiber draw tower based on a CO laser furnace
Open this publication in new window or tab >>Specialty optical fiber fabrication: fiber draw tower based on a CO laser furnace
Show others...
2021 (English)In: Journal of the Optical Society of America. B, Optical physics, ISSN 0740-3224, E-ISSN 1520-8540, Vol. 38, no 12, p. F122-F129Article in journal (Refereed) Published
Abstract [en]

An experimental, laboratory-scale optical fiber drawing tower based on CO laser heating has been developed and used to fabricate speciality optical fiber. The CO laser was utilized in a symmetric four beam heating system. The localized and responsive heating time of the laser-based furnace was beneficial for manufacturing crystalline core fibers, specifically, silicon core optical fibers. Moreover, the specific absorption properties of the CO laser radiation in silica have been evaluated with the aid of finite element modeling. In comparison to the more traditional CO2 laser, CO lasers were found to improve temperature uniformity and heating times while minimizing surface evaporation.

Place, publisher, year, edition, pages
The Optical Society, 2021
National Category
Atom and Molecular Physics and Optics
Identifiers
urn:nbn:se:kth:diva-306515 (URN)10.1364/JOSAB.437667 (DOI)000724531400015 ()2-s2.0-85120081360 (Scopus ID)
Note

QC 20211217

Available from: 2021-12-17 Created: 2021-12-17 Last updated: 2024-03-18Bibliographically approved
4. Mach-Zehnder Interferometer for In-Situ Non-Contact Temperature Monitoring During Thermal Processing of an Optical Fibre
Open this publication in new window or tab >>Mach-Zehnder Interferometer for In-Situ Non-Contact Temperature Monitoring During Thermal Processing of an Optical Fibre
2021 (English)In: Journal of Lightwave Technology, ISSN 0733-8724, E-ISSN 1558-2213, Vol. 39, no 22, p. 7223-7230Article in journal (Refereed) Published
Abstract [en]

A Mach-Zehnder interferometer is formed in the transverse plane of an optical fibre. This is exploited to monitor the temperature of any given optical fibre in real time, without any predesigned temperature sensing elements engineered into the fibre and without a need to access the fibre ends. The interferometer is formed by the refraction at the air-glass interface and the subsequent internal reflections within the fibre. The temperature response of the fibre is then measured by quadrature phase shift detection of the interference pattern. For context, this is compared to finite element modelling and a previously studied Fabry-Perot interferometer configuration. The temperature of an optical fibre was measured from room temperature up to 1174 degrees C with an error of +/- 2.6% for the Mach-Zehnder type interferometer. The measurement techniques presented offer a useful tool for precise temperature measurement for applications such as fibre post-processing.

Place, publisher, year, edition, pages
Institute of Electrical and Electronics Engineers (IEEE), 2021
Keywords
Optical fiber measurements, temperature measurement, laser materials-processing applications, interferometry
National Category
Atom and Molecular Physics and Optics
Identifiers
urn:nbn:se:kth:diva-305334 (URN)10.1109/JLT.2021.3109462 (DOI)000716698300022 ()2-s2.0-85114744567 (Scopus ID)
Note

QC 20211130

Available from: 2021-11-30 Created: 2021-11-30 Last updated: 2022-06-25Bibliographically approved
5. Temperature dynamics in silicon core fibers during CO2 laser processing
Open this publication in new window or tab >>Temperature dynamics in silicon core fibers during CO2 laser processing
2022 (English)In: Optics Express, E-ISSN 1094-4087, Vol. 30, no 1, p. 92-100Article in journal (Refereed) Published
Abstract [en]

Silicon core fibers are a promising candidate for optoelectronic and photonic applications. Fabrication and post-processing of those fibers is thus far done without precise knowledge of the processing temperatures. Here, a simple technique is presented that allows for in-situ temperature monitoring during thermal processing of silicon core fibers. The temperature was probed across the silicon melting point and cooling rates above 3500 degrees C s(-1) were measured. The silicon core was found to be molten at a temperature of 1281 degrees C, more than 100 degrees C below the bulk silicon melting point. This is attributed to stress inbuilt to silicon core fibers during the fabrication process.

Place, publisher, year, edition, pages
The Optical Society, 2022
National Category
Atom and Molecular Physics and Optics
Research subject
Physics
Identifiers
urn:nbn:se:kth:diva-307099 (URN)10.1364/oe.445774 (DOI)000738278500008 ()35201197 (PubMedID)2-s2.0-85122256507 (Scopus ID)
Funder
Swedish Foundation for Strategic Research , RMA15-0135
Note

QC 20220124

Available from: 2022-01-11 Created: 2022-01-11 Last updated: 2022-09-15Bibliographically approved

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