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Precipitation kinetics of ferritic / martensitic oxide dispersion strengthened steels: Influence of the matrix phase transformation
KTH, School of Industrial Engineering and Management (ITM), Materials Science and Engineering, Properties. Université Paris-Saclay, CEA, Service de Recherche en Matériaux et procédés Avancés, 91191, Gif-sur-Yvette, France.ORCID iD: 0000-0001-7096-1200
Université Paris-Saclay, CEA, Service de Recherche en Matériaux et procédés Avancés, 91191, Gif-sur-Yvette, France.
Univ. Grenoble Alpes, CNRS, Grenoble INP, SIMAP, F-38000, Grenoble, France.
Université Paris-Saclay, CEA, Service de Recherche en Matériaux et procédés Avancés, 91191, Gif-sur-Yvette, France; Univ. Grenoble Alpes, CNRS, Grenoble INP, SIMAP, F-38000, Grenoble, France.
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2024 (English)In: Acta Materialia, ISSN 1359-6454, E-ISSN 1873-2453, Vol. 280, article id 120328Article in journal (Refereed) Published
Abstract [en]

ODS steels are candidate materials for the future generation of nuclear power plants. Ferritic / Martensitic (F/M) ODS steels display better formability thanks to high temperature austenitic transformation. The precipitation kinetics of a F/M Fe‑9Cr ODS steel during powder consolidation up to 1100 °C has been characterized by in‑situ Small Angle X-ray Scattering (SAXS). The influence of the matrix phase transformation has been established, showing an increase of the growth rate of the nano‑oxides in austenite, leading to nano‑oxides ∼ 2x larger in diameter than in Fe‑14Cr ferritic ODS grades at the end of the thermal treatment. These results are further supported by local atom probe tomography (APT) performed across grains showing contrasted microstructure and composition. Anomalous SAXS as well as comparison between APT and SAXS provide evidence that the nano‑oxides stabilize with a Y2Ti2O7 or Y2TiO5 stoichiometry around 1100 °C.

Place, publisher, year, edition, pages
Elsevier BV , 2024. Vol. 280, article id 120328
Keywords [en]
Atom probe tomography (APT), Ferritic/Martensitic steel, Nano-oxides, ODS steel, Precipitation, Small angle X-ray, scattering (SAXS)
National Category
Metallurgy and Metallic Materials
Identifiers
URN: urn:nbn:se:kth:diva-353468DOI: 10.1016/j.actamat.2024.120328ISI: 001388571600001Scopus ID: 2-s2.0-85202526809OAI: oai:DiVA.org:kth-353468DiVA, id: diva2:1899143
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QC 20250122

Available from: 2024-09-19 Created: 2024-09-19 Last updated: 2025-01-22Bibliographically approved

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Spartacus, Gabriel

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